File: D:\DATA\20130207\CO130208_01.D Operator: PBS Date Acquired: 8 Feb 2013 14:30 Instrument: 7890A_5975C Method File: 5PSPLITLESS20.M Sample Name: DEHP 0 ug/ml Misc Info: Vial Number : 140 TIC: CO130208_01.D\data.ms DEHP 0 ug/ml time counts time counts time counts time counts 5.093 11805 5.159 10666 5.224 18489 5.289 13455 5.099 12970 5.165 11202 5.230 18266 5.295 12359 5.105 12681 5.170 11685 5.236 15278 5.301 12730 5.111 12427 5.176 11696 5.242 15566 5.307 12743 5.117 11665 5.182 11183 5.248 14708 5.313 13029 5.123 11274 5.188 11067 5.254 15260 5.319 12150 5.129 11477 5.194 11151 5.260 14045 5.325 10471 5.135 12749 5.200 11045 5.265 14457 5.331 10786 5.141 11795 5.206 13420 5.271 13937 5.337 10333 5.147 12288 5.212 14486 5.277 13396 5.343 9565 5.153 12116 5.218 17758 5.283 13542 5.349 9450 TIC: CO130208_01.D\data.ms DEHP 0 ug/ml time counts time counts time counts time counts 5.354 10040 5.420 9350 5.485 11000 5.550 10586 5.360 10243 5.426 9647 5.491 10655 5.556 10048 5.366 10928 5.432 10125 5.497 11438 5.562 10882 5.372 9893 5.438 11232 5.503 11622 5.568 11272 5.378 10597 5.444 9975 5.509 11462 5.574 12922 5.384 10701 5.449 10327 5.515 11313 5.580 13487 5.390 11110 5.455 9916 5.521 11664 5.586 12363 5.396 10410 5.461 9651 5.527 10380 5.592 11271 5.402 9513 5.467 9392 5.533 10341 5.598 12274 5.408 9693 5.473 10562 5.538 10613 5.604 11190 5.414 10096 5.479 10166 5.544 10390 5.610 10622 TIC: CO130208_01.D\data.ms DEHP 0 ug/ml time counts time counts time counts time counts 5.616 10951 5.681 10603 5.746 11666 5.812 10071 5.622 10723 5.687 9989 5.752 9275 5.817 9870 5.628 9857 5.693 9234 5.758 11354 5.823 10590 5.633 11415 5.699 10065 5.764 10476 5.829 10919 5.639 10732 5.705 10906 5.770 10361 5.835 10420 5.645 10407 5.711 10949 5.776 9524 5.841 10945 5.651 10631 5.717 10034 5.782 10298 5.847 11515 5.657 10488 5.722 11152 5.788 10590 5.853 11123 5.663 9810 5.728 10920 5.794 9870 5.859 12053 5.669 10296 5.734 11208 5.800 9399 5.865 12076 5.675 10884 5.740 10969 5.806 9783 5.871 11861 TIC: CO130208_01.D\data.ms DEHP 0 ug/ml time counts time counts time counts time counts 5.877 11726 5.942 11619 6.007 11732 6.073 11489 5.883 11225 5.948 11655 6.013 11581 6.079 10821 5.889 10956 5.954 11880 6.019 11778 6.085 10115 5.895 11142 5.960 11535 6.025 11648 6.090 11213 5.901 10930 5.966 12533 6.031 11872 6.096 10135 5.906 12088 5.972 11375 6.037 10859 6.102 10565 5.912 13424 5.978 10852 6.043 12154 6.108 11477 5.918 13530 5.984 11388 6.049 11133 6.114 10655 5.924 12773 5.990 11584 6.055 11479 6.120 11596 5.930 12233 5.996 11932 6.061 11409 6.126 11104 5.936 12694 6.001 10973 6.067 11735 6.132 10859 TIC: CO130208_01.D\data.ms DEHP 0 ug/ml time counts time counts time counts time counts 6.138 11012 6.203 11863 6.269 11216 6.334 13802 6.144 10835 6.209 12355 6.274 12448 6.340 13215 6.150 10579 6.215 12002 6.280 12350 6.346 13045 6.156 11153 6.221 11811 6.286 12374 6.352 13132 6.162 10497 6.227 12646 6.292 12813 6.358 11702 6.168 11948 6.233 11917 6.298 12506 6.363 13247 6.174 12631 6.239 12188 6.304 12631 6.369 13152 6.179 12451 6.245 12051 6.310 12215 6.375 13290 6.185 11371 6.251 12315 6.316 11633 6.381 12778 6.191 11260 6.257 12599 6.322 11940 6.387 13926 6.197 11539 6.263 11803 6.328 13090 6.393 14560 TIC: CO130208_01.D\data.ms DEHP 0 ug/ml time counts time counts time counts time counts 6.399 14175 6.464 15410 6.530 14096 6.595 13774 6.405 14341 6.470 15238 6.536 14189 6.601 15632 6.411 13546 6.476 14869 6.542 15232 6.607 15100 6.417 14373 6.482 15217 6.547 15648 6.613 16063 6.423 13034 6.488 15276 6.553 13543 6.619 16502 6.429 13306 6.494 16099 6.559 14682 6.625 15427 6.435 14043 6.500 14230 6.565 14434 6.631 15542 6.441 13900 6.506 14803 6.571 15813 6.637 16004 6.447 14956 6.512 15219 6.577 14174 6.642 15670 6.453 15334 6.518 15296 6.583 14290 6.648 16071 6.458 15550 6.524 13820 6.589 14613 6.654 16384 TIC: CO130208_01.D\data.ms DEHP 0 ug/ml time counts time counts time counts time counts 6.660 15475 6.726 35625 6.791 18998 6.856 18849 6.666 16525 6.731 32145 6.797 19656 6.862 17392 6.672 14552 6.737 29038 6.803 19097 6.868 18484 6.678 15816 6.743 25368 6.809 17314 6.874 17516 6.684 16781 6.749 23556 6.815 17422 6.880 18516 6.690 17404 6.755 20195 6.821 17639 6.886 20440 6.696 17817 6.761 19664 6.826 19051 6.892 19174 6.702 19197 6.767 18842 6.832 19536 6.898 19186 6.708 22870 6.773 19854 6.838 18774 6.904 20038 6.714 28510 6.779 20377 6.844 18633 6.910 19549 6.720 34578 6.785 19216 6.850 17122 6.915 19814 TIC: CO130208_01.D\data.ms DEHP 0 ug/ml time counts time counts time counts time counts 6.921 19824 6.987 18357 7.052 19387 7.117 20283 6.927 18913 6.993 19274 7.058 19836 7.123 20329 6.933 20190 6.999 19271 7.064 18722 7.129 20682 6.939 19696 7.005 18696 7.070 18408 7.135 20815 6.945 18219 7.010 18808 7.076 17623 7.141 20456 6.951 18951 7.016 19355 7.082 19208 7.147 21229 6.957 17575 7.022 18752 7.088 19438 7.153 19734 6.963 18436 7.028 18946 7.094 20135 7.159 21418 6.969 19257 7.034 19164 7.099 17898 7.165 22018 6.975 19297 7.040 19113 7.105 19049 7.171 21585 6.981 18941 7.046 18469 7.111 20543 7.177 20856 TIC: CO130208_01.D\data.ms DEHP 0 ug/ml time counts time counts time counts time counts 7.183 22066 7.248 24535 7.313 25811 7.378 24456 7.188 21578 7.254 23625 7.319 24453 7.384 24311 7.194 22608 7.260 21159 7.325 24551 7.390 24558 7.200 23191 7.266 22086 7.331 24110 7.396 25891 7.206 23701 7.272 21037 7.337 25404 7.402 23835 7.212 22223 7.278 21654 7.343 22794 7.408 24342 7.218 24088 7.283 21455 7.349 25400 7.414 23880 7.224 22240 7.289 23944 7.355 26235 7.420 25294 7.230 22149 7.295 24273 7.361 24424 7.426 26206 7.236 23275 7.301 26188 7.367 25266 7.432 27637 7.242 21760 7.307 25034 7.372 25511 7.438 25354 TIC: CO130208_01.D\data.ms DEHP 0 ug/ml time counts time counts time counts time counts 7.444 23856 7.509 26887 7.574 30487 7.640 31454 7.450 25231 7.515 27527 7.580 32899 7.646 32126 7.456 24924 7.521 26306 7.586 32352 7.651 32792 7.462 25901 7.527 27811 7.592 29861 7.657 30516 7.467 26375 7.533 30172 7.598 30603 7.663 31366 7.473 25336 7.539 30542 7.604 31053 7.669 29850 7.479 26861 7.545 30555 7.610 32350 7.675 29733 7.485 27372 7.551 29512 7.616 30360 7.681 29338 7.491 27721 7.556 29600 7.622 31573 7.687 32126 7.497 27971 7.562 29713 7.628 32485 7.693 31286 7.503 26199 7.568 31455 7.634 32309 7.699 29396 TIC: CO130208_01.D\data.ms DEHP 0 ug/ml time counts time counts time counts time counts 7.705 30102 7.770 32843 7.835 37858 7.901 36840 7.711 31555 7.776 31429 7.841 37292 7.907 35813 7.717 34149 7.782 32414 7.847 35938 7.913 34954 7.723 32632 7.788 33417 7.853 35809 7.919 37477 7.729 35747 7.794 32750 7.859 33626 7.924 40079 7.735 36659 7.800 32275 7.865 35894 7.930 42112 7.740 37677 7.806 34523 7.871 34839 7.936 44839 7.746 36419 7.812 33467 7.877 35045 7.942 46839 7.752 36009 7.818 34936 7.883 34524 7.948 50419 7.758 35027 7.824 34007 7.889 35667 7.954 46841 7.764 33399 7.830 36473 7.895 35147 7.960 45253 TIC: CO130208_01.D\data.ms DEHP 0 ug/ml time counts time counts time counts time counts 7.966 43418 8.031 39770 8.097 42529 8.162 43323 7.972 41782 8.037 39651 8.103 43331 8.168 45552 7.978 39583 8.043 38541 8.108 42670 8.174 43554 7.984 38675 8.049 39270 8.114 41918 8.180 42195 7.990 39261 8.055 44051 8.120 40865 8.186 42713 7.996 39334 8.061 56257 8.126 39090 8.192 44494 8.002 39234 8.067 66031 8.132 41609 8.197 44182 8.008 39226 8.073 67877 8.138 41087 8.203 45293 8.014 41265 8.079 55720 8.144 44446 8.209 47988 8.019 39827 8.085 48160 8.150 43535 8.215 49310 8.025 41752 8.091 42811 8.156 43809 8.221 48927 TIC: CO130208_01.D\data.ms DEHP 0 ug/ml time counts time counts time counts time counts 8.227 48817 8.292 52429 8.358 55318 8.423 57055 8.233 47304 8.298 52777 8.364 59202 8.429 54363 8.239 47673 8.304 51630 8.370 66610 8.435 54562 8.245 47701 8.310 49782 8.376 69268 8.441 55647 8.251 48213 8.316 49595 8.381 66767 8.447 53099 8.257 48748 8.322 46604 8.387 58473 8.453 51977 8.263 48644 8.328 50030 8.393 54404 8.459 54715 8.269 49104 8.334 51177 8.399 54032 8.465 54009 8.275 49079 8.340 51242 8.405 53401 8.471 52776 8.281 50725 8.346 50608 8.411 53586 8.476 53105 8.287 53638 8.352 51082 8.417 56758 8.482 55007 TIC: CO130208_01.D\data.ms DEHP 0 ug/ml time counts time counts time counts time counts 8.488 56025 8.554 56673 8.619 56323 8.684 62384 8.494 57511 8.560 56169 8.625 58889 8.690 61700 8.500 57013 8.565 59170 8.631 57765 8.696 64971 8.506 54803 8.571 59791 8.637 57359 8.702 66487 8.512 55771 8.577 59846 8.643 62177 8.708 65024 8.518 54428 8.583 60095 8.649 65596 8.714 67693 8.524 51811 8.589 59610 8.655 72459 8.720 65542 8.530 55602 8.595 62061 8.660 71927 8.726 63613 8.536 54876 8.601 58059 8.666 72917 8.732 62867 8.542 56578 8.607 59041 8.672 67814 8.738 63526 8.548 54525 8.613 59479 8.678 65538 8.744 63520 TIC: CO130208_01.D\data.ms DEHP 0 ug/ml time counts time counts time counts time counts 8.749 67733 8.815 67700 8.880 66744 8.945 72890 8.755 67912 8.821 67641 8.886 70055 8.951 72235 8.761 66037 8.827 68441 8.892 69734 8.957 69879 8.767 63850 8.833 73465 8.898 70530 8.963 73908 8.773 62422 8.838 72060 8.904 71921 8.969 74072 8.779 66233 8.844 69096 8.910 74005 8.975 74496 8.785 66207 8.850 68518 8.916 71899 8.981 71685 8.791 69927 8.856 66805 8.922 71196 8.987 71588 8.797 70551 8.862 66394 8.928 72180 8.993 72767 8.803 68758 8.868 66163 8.933 70631 8.999 72845 8.809 66059 8.874 66752 8.939 72671 9.005 73323 TIC: CO130208_01.D\data.ms DEHP 0 ug/ml time counts time counts time counts time counts 9.011 70938 9.076 77672 9.141 83107 9.207 80857 9.017 73982 9.082 77701 9.147 81603 9.212 76587 9.023 75161 9.088 79864 9.153 82675 9.218 82720 9.028 71981 9.094 81500 9.159 83457 9.224 90517 9.034 75667 9.100 82245 9.165 85537 9.230 100357 9.040 72952 9.106 78428 9.171 83546 9.236 108989 9.046 73103 9.112 81415 9.177 83729 9.242 102149 9.052 76821 9.117 90735 9.183 84347 9.248 91222 9.058 77604 9.123 98796 9.189 84127 9.254 82801 9.064 79774 9.129 98736 9.195 85065 9.260 79781 9.070 75613 9.135 90025 9.201 80434 9.266 82031 TIC: CO130208_01.D\data.ms DEHP 0 ug/ml time counts time counts time counts time counts 9.272 77171 9.337 79642 9.402 82856 9.468 86052 9.278 77495 9.343 78093 9.408 85888 9.474 88155 9.284 77748 9.349 79536 9.414 81462 9.480 86842 9.290 79055 9.355 82250 9.420 83376 9.485 82324 9.296 81637 9.361 80941 9.426 83017 9.491 83480 9.301 83217 9.367 81741 9.432 83729 9.497 86013 9.307 86043 9.373 82141 9.438 85185 9.503 86866 9.313 82691 9.379 83368 9.444 85824 9.509 88289 9.319 78977 9.385 80434 9.450 87830 9.515 87469 9.325 79131 9.390 78648 9.456 89998 9.521 87334 9.331 79050 9.396 79125 9.462 87412 9.527 85924 TIC: CO130208_01.D\data.ms DEHP 0 ug/ml time counts time counts time counts time counts 9.533 81396 9.598 85499 9.664 91315 9.729 103931 9.539 81009 9.604 90127 9.669 98871 9.735 103994 9.545 82736 9.610 86767 9.675 99501 9.741 103917 9.551 83258 9.616 90236 9.681 99642 9.747 103753 9.557 84746 9.622 95154 9.687 101475 9.753 99790 9.563 82937 9.628 94693 9.693 103011 9.758 95555 9.569 80032 9.634 96349 9.699 107900 9.764 94625 9.574 84545 9.640 99170 9.705 106174 9.770 89224 9.580 83631 9.646 96889 9.711 103967 9.776 94111 9.586 89538 9.652 94087 9.717 99231 9.782 86726 9.592 86912 9.658 96342 9.723 103940 9.788 89324 TIC: CO130208_01.D\data.ms DEHP 0 ug/ml time counts time counts time counts time counts 9.794 89171 9.859 94917 9.925 93839 9.990 106965 9.800 92750 9.865 97509 9.931 94483 9.996 107181 9.806 88361 9.871 97410 9.937 96924 10.002 116222 9.812 92555 9.877 99196 9.942 98567 10.008 143283 9.818 92984 9.883 97952 9.948 96945 10.014 182055 9.824 89925 9.889 99273 9.954 96640 10.020 181798 9.830 91295 9.895 98832 9.960 98709 10.026 155153 9.836 93532 9.901 96316 9.966 98390 10.032 127777 9.842 92177 9.907 95879 9.972 101638 10.037 118512 9.848 93073 9.913 95108 9.978 103652 10.043 110521 9.853 92512 9.919 91669 9.984 106927 10.049 106954 TIC: CO130208_01.D\data.ms DEHP 0 ug/ml time counts time counts time counts time counts 10.055 105832 10.121 170967 10.186 114717 10.251 149039 10.061 100817 10.126 170885 10.192 113347 10.257 161842 10.067 99448 10.132 138816 10.198 117113 10.263 149699 10.073 98225 10.138 118758 10.204 113056 10.269 143843 10.079 99891 10.144 110494 10.210 109324 10.275 131107 10.085 101918 10.150 106673 10.216 109449 10.281 135387 10.091 100615 10.156 105169 10.221 105119 10.287 128290 10.097 103299 10.162 105487 10.227 111601 10.293 128882 10.103 104670 10.168 102901 10.233 108053 10.299 132927 10.109 119369 10.174 108025 10.239 113498 10.305 130344 10.115 146142 10.180 106032 10.245 122498 10.310 126913 TIC: CO130208_01.D\data.ms DEHP 0 ug/ml time counts time counts time counts time counts 10.316 130843 10.382 183126 10.447 192624 10.512 143934 10.322 144622 10.388 147407 10.453 187013 10.518 147265 10.328 141713 10.394 134619 10.459 165472 10.524 159500 10.334 129418 10.399 133396 10.465 145072 10.530 173530 10.340 119909 10.405 132982 10.471 137548 10.536 177788 10.346 120832 10.411 131649 10.477 143541 10.542 169519 10.352 125476 10.417 137309 10.483 170457 10.548 177325 10.358 159362 10.423 147517 10.489 201637 10.554 209348 10.364 210692 10.429 159369 10.494 223690 10.560 257754 10.370 258130 10.435 166667 10.500 194127 10.566 256486 10.376 236084 10.441 177423 10.506 159419 10.572 220564 TIC: CO130208_01.D\data.ms DEHP 0 ug/ml time counts time counts time counts time counts 10.578 162112 10.643 126129 10.708 147819 10.773 284363 10.583 142556 10.649 131944 10.714 162165 10.779 296060 10.589 132734 10.655 144697 10.720 191474 10.785 311245 10.595 133945 10.661 152048 10.726 226153 10.791 345095 10.601 138746 10.667 148854 10.732 232350 10.797 334137 10.607 148623 10.673 142208 10.738 205615 10.803 262914 10.613 159353 10.678 146876 10.744 169085 10.809 193041 10.619 156842 10.684 148139 10.750 150588 10.815 145965 10.625 140498 10.690 140893 10.756 156945 10.821 136665 10.631 133077 10.696 135587 10.762 190945 10.827 129677 10.637 124797 10.702 136250 10.767 246574 10.833 127677 TIC: CO130208_01.D\data.ms DEHP 0 ug/ml time counts time counts time counts time counts 10.839 120519 10.904 166675 10.969 190456 11.035 619636 10.845 124689 10.910 151204 10.975 235238 11.041 582979 10.851 124920 10.916 150960 10.981 267909 11.046 448322 10.857 130355 10.922 147929 10.987 264453 11.052 287497 10.862 141751 10.928 148429 10.993 232290 11.058 198513 10.868 161241 10.934 147480 10.999 212662 11.064 164761 10.874 204989 10.940 146248 11.005 237368 11.070 160072 10.880 250250 10.946 139840 11.011 291687 11.076 158775 10.886 257578 10.951 137813 11.017 366026 11.082 155568 10.892 234251 10.957 143601 11.023 452164 11.088 165391 10.898 195607 10.963 153033 11.029 557944 11.094 203573 TIC: CO130208_01.D\data.ms DEHP 0 ug/ml time counts time counts time counts time counts 11.100 252957 11.165 744710 11.230 212188 11.296 447438 11.106 276381 11.171 486143 11.236 199824 11.302 395138 11.112 253991 11.177 333224 11.242 188565 11.308 283607 11.118 212381 11.183 290095 11.248 180976 11.314 234024 11.124 197810 11.189 293570 11.254 194637 11.319 218099 11.130 228823 11.195 309576 11.260 253270 11.325 201258 11.135 309810 11.201 314398 11.266 329267 11.331 185592 11.141 436074 11.207 270344 11.272 349048 11.337 175701 11.147 557816 11.213 233988 11.278 303991 11.343 171911 11.153 753638 11.219 211371 11.284 290072 11.349 173691 11.159 853806 11.225 211484 11.290 371006 11.355 187879 TIC: CO130208_01.D\data.ms DEHP 0 ug/ml time counts time counts time counts time counts 11.361 215491 11.426 187573 11.492 205386 11.557 232982 11.367 247792 11.432 204847 11.498 206283 11.563 231859 11.373 260251 11.438 209793 11.503 220145 11.569 234204 11.379 241519 11.444 210447 11.509 234061 11.575 227606 11.385 211746 11.450 221189 11.515 232436 11.581 226409 11.391 195833 11.456 223901 11.521 221958 11.587 234050 11.397 182651 11.462 224463 11.527 210116 11.592 251669 11.403 181908 11.468 215454 11.533 212112 11.598 260860 11.409 186178 11.474 200712 11.539 211254 11.604 274777 11.414 191203 11.480 207020 11.545 214625 11.610 284496 11.420 188534 11.486 206910 11.551 222108 11.616 318619 TIC: CO130208_01.D\data.ms DEHP 0 ug/ml time counts time counts time counts time counts 11.622 378442 11.687 230704 11.753 374174 11.818 252147 11.628 447369 11.693 236145 11.759 454254 11.824 242230 11.634 504870 11.699 246199 11.765 549416 11.830 241118 11.640 510101 11.705 247384 11.771 549360 11.836 237293 11.646 448794 11.711 252879 11.776 445630 11.842 239944 11.652 388085 11.717 260757 11.782 335395 11.848 251678 11.658 342722 11.723 271852 11.788 276279 11.854 255276 11.664 332180 11.729 283105 11.794 255154 11.860 264692 11.670 296084 11.735 297889 11.800 248040 11.866 263592 11.676 253646 11.741 316063 11.806 239751 11.871 256693 11.682 229592 11.747 336801 11.812 251954 11.877 253955 TIC: CO130208_01.D\data.ms DEHP 0 ug/ml time counts time counts time counts time counts 11.883 250696 11.949 236921 12.014 274083 12.079 256164 11.889 240078 11.955 244480 12.020 272527 12.085 274811 11.895 236246 11.960 257823 12.026 266225 12.091 272068 11.901 239183 11.966 262603 12.032 261737 12.097 271887 11.907 240151 11.972 260396 12.038 251711 12.103 268282 11.913 240104 11.978 247449 12.044 251038 12.109 264193 11.919 229754 11.984 249039 12.050 254468 12.115 263803 11.925 232793 11.990 253475 12.055 252635 12.121 261361 11.931 231251 11.996 264848 12.061 250595 12.127 255039 11.937 238367 12.002 284967 12.067 248358 12.133 258380 11.943 238019 12.008 282257 12.073 250791 12.139 255527 TIC: CO130208_01.D\data.ms DEHP 0 ug/ml time counts time counts time counts time counts 12.144 248370 12.210 335165 12.275 265810 12.340 261790 12.150 251449 12.216 308573 12.281 264879 12.346 265498 12.156 251887 12.222 285736 12.287 269421 12.352 272093 12.162 246937 12.228 270550 12.293 282125 12.358 283153 12.168 242751 12.234 267382 12.299 291795 12.364 301148 12.174 247221 12.239 266861 12.305 311076 12.370 302746 12.180 246706 12.245 255519 12.311 305573 12.376 294330 12.186 250484 12.251 261939 12.317 301732 12.382 283481 12.192 259576 12.257 263977 12.323 287257 12.388 281626 12.198 280227 12.263 267411 12.328 273824 12.394 271642 12.204 306270 12.269 267147 12.334 264605 12.400 268003 TIC: CO130208_01.D\data.ms DEHP 0 ug/ml time counts time counts time counts time counts 12.406 261571 12.471 264628 12.536 258041 12.601 259800 12.412 266267 12.477 250123 12.542 263476 12.607 256691 12.418 276830 12.483 248009 12.548 260295 12.613 256169 12.423 269485 12.489 251859 12.554 264593 12.619 258431 12.429 266662 12.495 256934 12.560 261729 12.625 255767 12.435 265145 12.501 254465 12.566 252111 12.631 251344 12.441 278736 12.507 254637 12.572 258178 12.637 253385 12.447 291058 12.512 248844 12.578 256319 12.643 248996 12.453 299510 12.518 252475 12.584 264208 12.649 252855 12.459 301378 12.524 250107 12.590 266788 12.655 250164 12.465 280861 12.530 249092 12.596 260150 12.661 250165 TIC: CO130208_01.D\data.ms DEHP 0 ug/ml time counts time counts time counts time counts 12.667 254439 12.732 243708 12.797 241855 12.863 406876 12.673 249483 12.738 251120 12.803 240456 12.869 482267 12.679 245125 12.744 261261 12.809 244821 12.875 504295 12.685 247651 12.750 282786 12.815 251431 12.880 461003 12.691 243888 12.756 310692 12.821 250289 12.886 377270 12.696 243604 12.762 328816 12.827 244714 12.892 307545 12.702 238691 12.768 312712 12.833 247786 12.898 263691 12.708 237441 12.774 283958 12.839 247850 12.904 252150 12.714 242663 12.780 255928 12.845 256627 12.910 244726 12.720 240678 12.785 242108 12.851 286842 12.916 239687 12.726 242449 12.791 244681 12.857 347335 12.922 234996 TIC: CO130208_01.D\data.ms DEHP 0 ug/ml time counts time counts time counts time counts 12.928 235794 12.993 236200 13.059 223398 13.124 213492 12.934 236562 12.999 236049 13.064 225344 13.130 213731 12.940 247561 13.005 234454 13.070 224124 13.136 215814 12.946 270308 13.011 235925 13.076 222647 13.142 220585 12.952 297486 13.017 230841 13.082 221591 13.148 224371 12.958 310860 13.023 226932 13.088 225469 13.153 225417 12.964 296554 13.029 227979 13.094 227503 13.159 229018 12.969 276350 13.035 218874 13.100 227539 13.165 228240 12.975 255238 13.041 225458 13.106 225715 13.171 219189 12.981 237545 13.047 223321 13.112 223073 13.177 216586 12.987 239785 13.053 219478 13.118 220068 13.183 211813 TIC: CO130208_01.D\data.ms DEHP 0 ug/ml time counts time counts time counts time counts 13.189 214654 13.254 206004 13.320 230210 13.385 209373 13.195 210849 13.260 211852 13.326 222267 13.391 202775 13.201 211908 13.266 210237 13.332 221962 13.397 204869 13.207 210535 13.272 216062 13.337 216406 13.403 201684 13.213 214581 13.278 221878 13.343 210337 13.409 204581 13.219 211667 13.284 238946 13.349 227715 13.415 198191 13.225 211663 13.290 282911 13.355 239695 13.421 205918 13.231 212221 13.296 310030 13.361 239912 13.427 199887 13.237 210492 13.302 296863 13.367 237899 13.432 200466 13.243 202703 13.308 269492 13.373 227942 13.438 208812 13.248 204240 13.314 255362 13.379 215323 13.444 202200 TIC: CO130208_01.D\data.ms DEHP 0 ug/ml time counts time counts time counts time counts 13.450 198065 13.516 201984 13.581 203176 13.646 224463 13.456 202658 13.521 196148 13.587 205182 13.652 213859 13.462 198677 13.527 198779 13.593 211032 13.658 218073 13.468 202432 13.533 198269 13.599 238280 13.664 211927 13.474 204406 13.539 197212 13.605 353318 13.670 210711 13.480 201428 13.545 202702 13.610 680775 13.676 211468 13.486 205735 13.551 197268 13.616 924181 13.682 210016 13.492 201368 13.557 195824 13.622 792665 13.688 201461 13.498 200489 13.563 200063 13.628 518752 13.694 204198 13.504 204856 13.569 200657 13.634 334083 13.700 200646 13.510 200432 13.575 202412 13.640 253818 13.705 199169 TIC: CO130208_01.D\data.ms DEHP 0 ug/ml time counts time counts time counts time counts 13.711 201230 13.777 194477 13.842 198862 13.907 218926 13.717 194286 13.783 197260 13.848 196073 13.913 212411 13.723 193733 13.789 204930 13.854 202053 13.919 202049 13.729 196836 13.794 212581 13.860 199280 13.925 191404 13.735 202060 13.800 230736 13.866 199272 13.931 191206 13.741 198999 13.806 258119 13.872 200472 13.937 186753 13.747 196992 13.812 266354 13.878 194342 13.943 190858 13.753 203282 13.818 247160 13.884 195545 13.949 190076 13.759 195815 13.824 233207 13.889 194314 13.955 187227 13.765 189738 13.830 219635 13.895 201385 13.961 192303 13.771 189936 13.836 213681 13.901 211716 13.967 192939 TIC: CO130208_01.D\data.ms DEHP 0 ug/ml time counts time counts time counts time counts 13.973 198387 14.038 245560 14.103 195094 14.168 222710 13.978 199196 14.044 223222 14.109 200849 14.174 307247 13.984 199109 14.050 203115 14.115 202301 14.180 571071 13.990 198153 14.056 201675 14.121 203190 14.186 1.026e+006 13.996 193981 14.062 195563 14.127 202190 14.192 1.19166e+006 14.002 188289 14.068 200319 14.133 197919 14.198 864017 14.008 196548 14.073 190736 14.139 191906 14.204 504700 14.014 197912 14.079 190984 14.145 191085 14.210 303648 14.020 207977 14.085 194075 14.151 196774 14.216 229209 14.026 222889 14.091 197489 14.157 192784 14.222 203070 14.032 244697 14.097 194371 14.162 195599 14.228 197849 TIC: CO130208_01.D\data.ms DEHP 0 ug/ml time counts time counts time counts time counts 14.234 194981 14.299 250878 14.364 199142 14.430 192136 14.240 195791 14.305 259071 14.370 200846 14.436 195848 14.246 197385 14.311 253104 14.376 205293 14.441 202854 14.252 196726 14.317 233615 14.382 196749 14.447 234476 14.257 199890 14.323 223403 14.388 198161 14.453 274849 14.263 202612 14.329 215606 14.394 190474 14.459 270818 14.269 212361 14.335 206420 14.400 188593 14.465 244045 14.275 229817 14.341 193039 14.406 197391 14.471 219316 14.281 243216 14.346 190432 14.412 203864 14.477 202362 14.287 247536 14.352 189672 14.418 206205 14.483 202819 14.293 245902 14.358 194982 14.424 203326 14.489 197362 TIC: CO130208_01.D\data.ms DEHP 0 ug/ml time counts time counts time counts time counts 14.495 198050 14.560 197906 14.625 191997 14.691 190805 14.501 200084 14.566 204748 14.631 193310 14.697 191334 14.507 191056 14.572 198433 14.637 191596 14.703 195193 14.513 196724 14.578 197814 14.643 187934 14.709 205438 14.519 202661 14.584 192821 14.649 186854 14.714 202836 14.525 196905 14.590 192381 14.655 184952 14.720 203514 14.530 201642 14.596 196659 14.661 187983 14.726 201619 14.536 201332 14.602 198041 14.667 190088 14.732 204927 14.542 195869 14.608 192743 14.673 187538 14.738 216060 14.548 200432 14.614 192314 14.679 188858 14.744 208441 14.554 198946 14.619 194059 14.685 190058 14.750 200919 TIC: CO130208_01.D\data.ms DEHP 0 ug/ml time counts time counts time counts time counts 14.756 193640 14.821 200914 14.887 182336 14.952 183182 14.762 198380 14.827 205933 14.893 184477 14.958 189123 14.768 203216 14.833 195942 14.898 195624 14.964 191050 14.774 217993 14.839 196146 14.904 193353 14.970 202107 14.780 224106 14.845 186913 14.910 197955 14.976 212961 14.786 227436 14.851 181793 14.916 196652 14.982 208357 14.792 216644 14.857 176854 14.922 191824 14.987 195592 14.798 211534 14.863 184910 14.928 190356 14.993 184664 14.803 204411 14.869 179554 14.934 186116 14.999 182597 14.809 199978 14.875 183327 14.940 185151 15.005 185173 14.815 196557 14.881 177186 14.946 187301 15.011 186215 TIC: CO130208_01.D\data.ms DEHP 0 ug/ml time counts time counts time counts time counts 15.017 188106 15.082 197088 15.148 178722 15.213 170210 15.023 191389 15.088 195529 15.154 183016 15.219 170776 15.029 205373 15.094 190190 15.160 182757 15.225 171615 15.035 203373 15.100 185059 15.166 176068 15.231 165969 15.041 198277 15.106 181656 15.171 175053 15.237 172795 15.047 188563 15.112 184232 15.177 170953 15.243 180909 15.053 183899 15.118 187465 15.183 166873 15.249 191307 15.059 184671 15.124 185769 15.189 168196 15.255 189023 15.065 183874 15.130 180232 15.195 168078 15.261 186390 15.071 188913 15.136 177136 15.201 169237 15.266 176955 15.077 186969 15.142 176047 15.207 171555 15.272 176743 TIC: CO130208_01.D\data.ms DEHP 0 ug/ml time counts time counts time counts time counts 15.278 188603 15.344 165336 15.409 158562 15.474 154647 15.284 195755 15.350 163138 15.415 161327 15.480 154603 15.290 187797 15.355 159444 15.421 158799 15.486 154796 15.296 185567 15.361 155545 15.427 158510 15.492 157476 15.302 176640 15.367 156193 15.433 161410 15.498 158713 15.308 174998 15.373 153894 15.439 161610 15.504 162827 15.314 170623 15.379 153664 15.445 160261 15.510 159698 15.320 172199 15.385 151460 15.450 156763 15.516 159319 15.326 175183 15.391 157430 15.456 157411 15.522 160668 15.332 174172 15.397 156822 15.462 157608 15.528 164136 15.338 167055 15.403 155147 15.468 156360 15.534 167147 TIC: CO130208_01.D\data.ms DEHP 0 ug/ml time counts time counts time counts time counts 15.539 166254 15.605 162858 15.670 166126 15.735 152128 15.545 167938 15.611 167785 15.676 162935 15.741 156661 15.551 165866 15.617 170801 15.682 161615 15.747 159835 15.557 177205 15.623 169756 15.688 155206 15.753 163947 15.563 183349 15.629 167805 15.694 155052 15.759 163341 15.569 187394 15.634 165712 15.700 150168 15.765 163554 15.575 180063 15.640 165508 15.706 149522 15.771 157753 15.581 172090 15.646 164553 15.712 150539 15.777 148973 15.587 161534 15.652 160042 15.718 153334 15.783 152807 15.593 156637 15.658 159416 15.723 152705 15.789 148641 15.599 159414 15.664 158700 15.729 151797 15.795 151008 TIC: CO130208_01.D\data.ms DEHP 0 ug/ml time counts time counts time counts time counts 15.801 148265 15.866 153452 15.931 146424 15.996 155128 15.807 144659 15.872 149075 15.937 146535 16.002 149004 15.812 148515 15.878 146417 15.943 146445 16.008 146662 15.818 148984 15.884 145481 15.949 142045 16.014 142323 15.824 149079 15.890 144253 15.955 142457 16.020 138515 15.830 149772 15.896 142622 15.961 143408 16.026 139303 15.836 149637 15.902 142930 15.967 140265 16.032 134690 15.842 157018 15.907 141754 15.973 141117 16.038 134647 15.848 154440 15.913 142070 15.979 144745 16.044 136565 15.854 156560 15.919 140761 15.985 150227 16.050 136704 15.860 157426 15.925 143384 15.991 148826 16.056 135846 TIC: CO130208_01.D\data.ms DEHP 0 ug/ml time counts time counts time counts time counts 16.062 135922 16.127 145866 16.192 135160 16.258 149669 16.068 137916 16.133 145014 16.198 141455 16.264 146746 16.074 141188 16.139 139095 16.204 140693 16.269 148767 16.080 144598 16.145 141439 16.210 137480 16.275 149720 16.086 151022 16.151 137939 16.216 143040 16.281 154017 16.091 149698 16.157 138411 16.222 154044 16.287 146368 16.097 147402 16.163 138121 16.228 160767 16.293 146207 16.103 148992 16.169 135554 16.234 172411 16.299 148102 16.109 147087 16.175 137023 16.240 178998 16.305 156678 16.115 143793 16.180 134333 16.246 173367 16.311 156939 16.121 145007 16.186 138189 16.252 155757 16.317 155734 TIC: CO130208_01.D\data.ms DEHP 0 ug/ml time counts time counts time counts time counts 16.323 152763 16.388 142758 16.454 129545 16.519 141073 16.329 152711 16.394 142811 16.459 130990 16.525 143173 16.335 159342 16.400 136321 16.465 130903 16.531 139452 16.341 158777 16.406 138025 16.471 132579 16.537 137324 16.347 159931 16.412 135938 16.477 134958 16.543 140338 16.353 163181 16.418 133036 16.483 135044 16.548 135361 16.359 161005 16.424 135967 16.489 135185 16.554 136298 16.364 161753 16.430 132228 16.495 137420 16.560 137381 16.370 156763 16.436 131228 16.501 140464 16.566 136864 16.376 152417 16.442 128602 16.507 139498 16.572 130597 16.382 148913 16.448 127685 16.513 142663 16.578 130621 TIC: CO130208_01.D\data.ms DEHP 0 ug/ml time counts time counts time counts time counts 16.584 131240 16.649 129246 16.715 120731 16.780 139193 16.590 134987 16.655 129817 16.721 123099 16.786 141474 16.596 139209 16.661 128482 16.727 121092 16.792 149496 16.602 138747 16.667 125294 16.732 118147 16.798 153928 16.608 141764 16.673 125151 16.738 120214 16.804 154746 16.614 145237 16.679 125343 16.744 117734 16.810 155804 16.620 140054 16.685 128125 16.750 122529 16.816 157568 16.626 135834 16.691 127115 16.756 121980 16.821 161863 16.632 135464 16.697 125734 16.762 124653 16.827 170330 16.637 134300 16.703 124238 16.768 127943 16.833 162721 16.643 133147 16.709 122510 16.774 130502 16.839 160925 TIC: CO130208_01.D\data.ms DEHP 0 ug/ml time counts time counts time counts time counts 16.845 148592 16.911 117188 16.976 130881 17.041 123563 16.851 137007 16.916 118645 16.982 131322 17.047 128724 16.857 132864 16.922 117253 16.988 132821 17.053 129149 16.863 131266 16.928 121979 16.994 131231 17.059 127617 16.869 129365 16.934 121398 17.000 128482 17.065 129242 16.875 124543 16.940 124850 17.005 133138 17.071 124941 16.881 125760 16.946 127054 17.011 131672 17.077 126476 16.887 126681 16.952 128780 17.017 129547 17.083 124385 16.893 123906 16.958 124710 17.023 129614 17.089 122379 16.899 121009 16.964 127139 17.029 129178 17.095 120027 16.905 120678 16.970 128257 17.035 124752 17.100 118050 TIC: CO130208_01.D\data.ms DEHP 0 ug/ml time counts time counts time counts time counts 17.106 114681 17.172 132431 17.237 116486 17.302 119807 17.112 114767 17.178 129662 17.243 112603 17.308 114781 17.118 118323 17.184 127740 17.249 113312 17.314 117154 17.124 124020 17.189 122780 17.255 115232 17.320 116513 17.130 123937 17.195 120544 17.261 114111 17.326 115652 17.136 126807 17.201 122209 17.267 119282 17.332 117699 17.142 125241 17.207 120849 17.273 118612 17.338 122246 17.148 125984 17.213 122181 17.278 120697 17.344 124247 17.154 128997 17.219 122057 17.284 121770 17.350 126013 17.160 127718 17.225 121420 17.290 123179 17.356 120481 17.166 129297 17.231 116448 17.296 122871 17.362 122747 TIC: CO130208_01.D\data.ms DEHP 0 ug/ml time counts time counts time counts time counts 17.368 122672 17.433 107920 17.498 104360 17.563 104170 17.373 124048 17.439 111208 17.504 102174 17.569 101834 17.379 122510 17.445 105860 17.510 103917 17.575 104884 17.385 118429 17.451 105286 17.516 103787 17.581 102112 17.391 120260 17.457 108301 17.522 101857 17.587 105428 17.397 118894 17.463 103760 17.528 102689 17.593 106630 17.403 116199 17.468 105705 17.534 102241 17.599 103775 17.409 113979 17.474 106025 17.540 107777 17.605 105079 17.415 111288 17.480 106611 17.546 103831 17.611 101349 17.421 108943 17.486 108400 17.552 102395 17.617 101177 17.427 109572 17.492 104342 17.557 101137 17.623 102792 TIC: CO130208_01.D\data.ms DEHP 0 ug/ml time counts time counts time counts time counts 17.629 102426 17.694 102035 17.759 108452 17.825 93668 17.635 103605 17.700 100572 17.765 106995 17.830 97825 17.641 101695 17.706 105289 17.771 104047 17.836 97453 17.647 103164 17.712 105545 17.777 104286 17.842 97114 17.652 101241 17.718 107489 17.783 102379 17.848 98322 17.658 103357 17.724 105589 17.789 99839 17.854 100193 17.664 103325 17.730 107217 17.795 103324 17.860 102211 17.670 105059 17.736 104578 17.801 103899 17.866 101871 17.676 101726 17.741 106283 17.807 102876 17.872 101156 17.682 102001 17.747 105353 17.813 100002 17.878 104288 17.688 104167 17.753 105591 17.819 97521 17.884 100343 TIC: CO130208_01.D\data.ms DEHP 0 ug/ml time counts time counts time counts time counts 17.890 99485 17.955 104511 18.020 100906 18.086 120744 17.896 101942 17.961 100336 18.026 103442 18.092 118356 17.902 104226 17.967 99018 18.032 103172 18.098 113921 17.908 102695 17.973 99410 18.038 107073 18.104 110932 17.914 104118 17.979 99300 18.044 108568 18.109 106769 17.920 104970 17.985 100586 18.050 112620 18.115 102139 17.925 104258 17.991 99451 18.056 108903 18.121 101169 17.931 104504 17.997 97921 18.062 111981 18.127 99692 17.937 104898 18.003 101094 18.068 115808 18.133 95821 17.943 102903 18.009 101760 18.074 115497 18.139 93889 17.949 102064 18.014 100263 18.080 120494 18.145 93092 TIC: CO130208_01.D\data.ms DEHP 0 ug/ml time counts time counts time counts time counts 18.151 94107 18.216 90380 18.282 93099 18.347 94462 18.157 94100 18.222 90151 18.288 90788 18.353 98302 18.163 96542 18.228 89610 18.293 92986 18.359 95447 18.169 94382 18.234 89053 18.299 95917 18.365 96344 18.175 92167 18.240 90537 18.305 95642 18.371 95260 18.181 87393 18.246 93189 18.311 92061 18.377 93104 18.187 92193 18.252 91280 18.317 94385 18.382 93656 18.193 92036 18.258 91968 18.323 95977 18.388 93768 18.198 89728 18.264 93811 18.329 92730 18.394 92698 18.204 89108 18.270 89347 18.335 94783 18.400 91561 18.210 89569 18.276 95444 18.341 94355 18.406 90034 TIC: CO130208_01.D\data.ms DEHP 0 ug/ml time counts time counts time counts time counts 18.412 88827 18.477 92457 18.543 91911 18.608 83654 18.418 86344 18.483 90980 18.549 89333 18.614 79417 18.424 87728 18.489 96843 18.555 87172 18.620 82307 18.430 89526 18.495 95189 18.561 85528 18.626 78464 18.436 88328 18.501 95577 18.566 85210 18.632 79581 18.442 91497 18.507 96625 18.572 85053 18.638 77342 18.448 90601 18.513 97593 18.578 84681 18.644 77368 18.454 92315 18.519 96237 18.584 83310 18.650 77416 18.460 88771 18.525 96652 18.590 82201 18.656 77752 18.466 91378 18.531 96916 18.596 85671 18.661 78284 18.472 92648 18.537 96156 18.602 82883 18.667 78048 TIC: CO130208_01.D\data.ms DEHP 0 ug/ml time counts time counts time counts time counts 18.673 78662 18.739 79648 18.804 79540 18.869 77669 18.679 75984 18.745 76806 18.810 77502 18.875 76391 18.685 77687 18.750 80147 18.816 78098 18.881 78850 18.691 78944 18.756 79389 18.822 78909 18.887 77791 18.697 80188 18.762 79690 18.828 78486 18.893 78419 18.703 82330 18.768 81561 18.834 79133 18.899 76502 18.709 80726 18.774 84244 18.840 78305 18.905 75798 18.715 79691 18.780 80775 18.845 77848 18.911 77427 18.721 81472 18.786 77874 18.851 77812 18.917 80931 18.727 81538 18.792 77731 18.857 78905 18.923 78451 18.733 80972 18.798 77584 18.863 77572 18.929 78000 TIC: CO130208_01.D\data.ms DEHP 0 ug/ml time counts time counts time counts time counts 18.934 78988 19.000 73141 19.065 75485 19.130 77700 18.940 77564 19.006 74113 19.071 74817 19.136 79010 18.946 77249 19.012 76351 19.077 76582 19.142 79976 18.952 78707 19.018 73055 19.083 74449 19.148 80461 18.958 77307 19.023 72575 19.089 78132 19.154 79544 18.964 77136 19.029 74264 19.095 76001 19.160 81099 18.970 76331 19.035 74528 19.101 75680 19.166 80848 18.976 78368 19.041 77483 19.107 77140 19.172 79443 18.982 75921 19.047 75684 19.113 76134 19.178 79695 18.988 76976 19.053 76327 19.118 76872 19.184 79561 18.994 76979 19.059 75476 19.124 76398 19.190 79115 TIC: CO130208_01.D\data.ms DEHP 0 ug/ml time counts time counts time counts time counts 19.196 79583 19.261 73635 19.326 71816 19.391 71074 19.202 78207 19.267 74233 19.332 75637 19.397 70053 19.207 77096 19.273 75188 19.338 75470 19.403 72709 19.213 78015 19.279 74755 19.344 71262 19.409 72095 19.219 79884 19.285 75932 19.350 72081 19.415 73548 19.225 75596 19.291 73184 19.356 70622 19.421 72796 19.231 75237 19.297 75400 19.362 70873 19.427 70712 19.237 75583 19.302 73409 19.368 72847 19.433 71933 19.243 75150 19.308 73922 19.374 73018 19.439 72535 19.249 72681 19.314 72522 19.380 70221 19.445 73867 19.255 72852 19.320 74972 19.386 72722 19.451 73057 TIC: CO130208_01.D\data.ms DEHP 0 ug/ml time counts time counts time counts time counts 19.457 73157 19.522 76466 19.587 76652 19.653 70763 19.463 73091 19.528 73357 19.593 78005 19.659 70712 19.469 70722 19.534 73012 19.599 75458 19.665 71323 19.475 73936 19.540 77204 19.605 74572 19.670 73340 19.480 73245 19.546 76822 19.611 74498 19.676 69448 19.486 70625 19.552 78662 19.617 73787 19.682 70045 19.492 71912 19.558 77308 19.623 70108 19.688 70423 19.498 74168 19.564 77044 19.629 70555 19.694 69540 19.504 75191 19.570 79558 19.635 71211 19.700 70254 19.510 75043 19.575 76948 19.641 67954 19.706 71695 19.516 75530 19.581 78195 19.647 72084 19.712 69692 TIC: CO130208_01.D\data.ms DEHP 0 ug/ml time counts time counts time counts time counts 19.718 70119 19.783 67369 19.849 69803 19.914 69679 19.724 69327 19.789 68219 19.854 70599 19.920 69098 19.730 67903 19.795 68208 19.860 67998 19.926 71838 19.736 68841 19.801 71002 19.866 69000 19.932 69064 19.742 66890 19.807 68926 19.872 72046 19.938 70429 19.748 70873 19.813 70349 19.878 69058 19.943 68956 19.754 68528 19.819 69378 19.884 67168 19.949 70715 19.759 68702 19.825 68863 19.890 68592 19.955 69431 19.765 68564 19.831 70436 19.896 66955 19.961 68848 19.771 67776 19.837 69387 19.902 69562 19.967 67835 19.777 71274 19.843 69575 19.908 69435 19.973 69504 TIC: CO130208_01.D\data.ms DEHP 0 ug/ml time counts time counts time counts time counts 19.979 67617 19.985 68108 19.991 66581