File: D:\DATA\20130207\CO130208_12.D Operator: PBS Date Acquired: 9 Feb 2013 13:04 Instrument: 7890A_5975C Method File: 5PSPLITLESS20.M Sample Name: DEHP 0 ug/ml Misc Info: Vial Number : 140 TIC: CO130208_12.D\data.ms DEHP 0 ug/ml time counts time counts time counts time counts 5.093 10419 5.159 11612 5.224 13873 5.289 12427 5.099 10817 5.164 11006 5.230 14573 5.295 13885 5.105 10178 5.170 11879 5.236 13603 5.301 12484 5.111 10226 5.176 11747 5.242 13769 5.307 12249 5.117 9159 5.182 12188 5.248 13139 5.313 12504 5.123 9637 5.188 12060 5.253 12694 5.319 11996 5.129 11233 5.194 10520 5.259 13491 5.325 11715 5.135 10756 5.200 10760 5.265 13131 5.331 10530 5.141 10218 5.206 11826 5.271 13489 5.337 10393 5.147 10442 5.212 12963 5.277 12579 5.342 11080 5.153 11065 5.218 14253 5.283 14293 5.348 11072 TIC: CO130208_12.D\data.ms DEHP 0 ug/ml time counts time counts time counts time counts 5.354 11512 5.420 11958 5.485 11619 5.550 12866 5.360 10655 5.426 11221 5.491 12410 5.556 12158 5.366 12102 5.432 11315 5.497 13019 5.562 12249 5.372 11309 5.437 10997 5.503 12341 5.568 12566 5.378 11481 5.443 10528 5.509 13508 5.574 14697 5.384 11089 5.449 11640 5.515 12561 5.580 14926 5.390 10385 5.455 11298 5.521 11965 5.586 15058 5.396 11572 5.461 12108 5.526 12576 5.592 13544 5.402 11399 5.467 11812 5.532 12912 5.598 13087 5.408 11285 5.473 11979 5.538 12831 5.604 12556 5.414 12043 5.479 12238 5.544 11854 5.610 13229 TIC: CO130208_12.D\data.ms DEHP 0 ug/ml time counts time counts time counts time counts 5.616 13940 5.681 12170 5.746 12949 5.811 12373 5.621 12196 5.687 12849 5.752 11971 5.817 12660 5.627 13271 5.693 11652 5.758 11899 5.823 13676 5.633 13159 5.699 12557 5.764 11854 5.829 12182 5.639 13028 5.705 11806 5.770 12728 5.835 11893 5.645 11712 5.710 12173 5.776 11803 5.841 12201 5.651 11812 5.716 13312 5.782 12450 5.847 13675 5.657 12571 5.722 13045 5.788 11509 5.853 13214 5.663 12319 5.728 13140 5.794 11685 5.859 12422 5.669 12097 5.734 12568 5.800 12513 5.865 12780 5.675 12277 5.740 12906 5.805 11103 5.871 12964 TIC: CO130208_12.D\data.ms DEHP 0 ug/ml time counts time counts time counts time counts 5.877 11582 5.942 13181 6.007 13861 6.073 12956 5.883 12417 5.948 13437 6.013 14072 6.078 13732 5.889 12655 5.954 14283 6.019 14016 6.084 13888 5.894 12026 5.960 13671 6.025 13741 6.090 13964 5.900 11996 5.966 13474 6.031 13343 6.096 13667 5.906 12890 5.972 12662 6.037 13638 6.102 14462 5.912 13431 5.978 13068 6.043 12499 6.108 13209 5.918 13648 5.984 13410 6.049 13423 6.114 14284 5.924 13910 5.989 13951 6.055 14775 6.120 13833 5.930 13832 5.995 13311 6.061 14381 6.126 12533 5.936 13770 6.001 13183 6.067 14070 6.132 14320 TIC: CO130208_12.D\data.ms DEHP 0 ug/ml time counts time counts time counts time counts 6.138 12803 6.203 14333 6.268 14187 6.334 16154 6.144 13760 6.209 13921 6.274 14487 6.340 14383 6.150 14174 6.215 13283 6.280 15255 6.346 15820 6.156 13328 6.221 13786 6.286 14970 6.351 15793 6.162 13786 6.227 14248 6.292 15229 6.357 16559 6.168 13582 6.233 15222 6.298 16398 6.363 15738 6.173 13451 6.239 14822 6.304 14634 6.369 17319 6.179 14250 6.245 15480 6.310 15390 6.375 17033 6.185 14883 6.251 15500 6.316 16207 6.381 15487 6.191 14943 6.257 14343 6.322 15049 6.387 17125 6.197 14744 6.262 14696 6.328 15891 6.393 15903 TIC: CO130208_12.D\data.ms DEHP 0 ug/ml time counts time counts time counts time counts 6.399 17475 6.464 19853 6.530 16341 6.595 17540 6.405 17516 6.470 19716 6.535 17572 6.601 18216 6.411 18333 6.476 18197 6.541 16643 6.607 17627 6.417 16719 6.482 18128 6.547 18243 6.613 18459 6.423 16738 6.488 17815 6.553 18278 6.619 18371 6.429 17718 6.494 18246 6.559 17118 6.625 18741 6.435 17527 6.500 18695 6.565 18298 6.630 19751 6.441 18619 6.506 17258 6.571 18187 6.636 19578 6.446 18325 6.512 17368 6.577 17634 6.642 18300 6.452 18321 6.518 18066 6.583 18665 6.648 18911 6.458 19405 6.524 18134 6.589 17285 6.654 17901 TIC: CO130208_12.D\data.ms DEHP 0 ug/ml time counts time counts time counts time counts 6.660 19054 6.725 36566 6.791 24004 6.856 22721 6.666 20106 6.731 30912 6.797 22819 6.862 21961 6.672 21546 6.737 30847 6.803 21809 6.868 23045 6.678 20253 6.743 27033 6.809 23335 6.874 23403 6.684 19888 6.749 24494 6.814 24234 6.880 23255 6.690 20219 6.755 24202 6.820 23343 6.886 23641 6.696 21168 6.761 24365 6.826 22433 6.892 23590 6.702 23059 6.767 23432 6.832 22057 6.898 25309 6.708 25403 6.773 23134 6.838 22517 6.903 23406 6.714 30845 6.779 23290 6.844 23646 6.909 24652 6.719 35540 6.785 23367 6.850 23625 6.915 22100 TIC: CO130208_12.D\data.ms DEHP 0 ug/ml time counts time counts time counts time counts 6.921 22956 6.987 23293 7.052 23403 7.117 26511 6.927 24067 6.993 24314 7.058 23430 7.123 26536 6.933 23520 6.998 22122 7.064 22370 7.129 25225 6.939 22621 7.004 24304 7.070 22544 7.135 24099 6.945 23533 7.010 23677 7.076 22164 7.141 25229 6.951 23122 7.016 22656 7.082 22127 7.147 25047 6.957 25005 7.022 22592 7.087 23272 7.153 24403 6.963 23722 7.028 23523 7.093 23061 7.159 26585 6.969 22574 7.034 22933 7.099 23138 7.165 27843 6.975 23572 7.040 23467 7.105 25062 7.171 28111 6.981 23575 7.046 23219 7.111 24998 7.177 28865 TIC: CO130208_12.D\data.ms DEHP 0 ug/ml time counts time counts time counts time counts 7.182 27444 7.248 29247 7.313 33048 7.378 32654 7.188 28509 7.254 29564 7.319 32556 7.384 32091 7.194 28411 7.260 30104 7.325 32877 7.390 31916 7.200 28192 7.266 29091 7.331 32957 7.396 33517 7.206 28458 7.271 28352 7.337 33364 7.402 32324 7.212 29622 7.277 29428 7.343 30966 7.408 32830 7.218 27943 7.283 31363 7.349 31485 7.414 32658 7.224 29687 7.289 31314 7.355 30540 7.420 31720 7.230 28846 7.295 32640 7.360 32282 7.426 32557 7.236 28809 7.301 33312 7.366 31506 7.432 32360 7.242 29820 7.307 33874 7.372 29667 7.438 31440 TIC: CO130208_12.D\data.ms DEHP 0 ug/ml time counts time counts time counts time counts 7.444 32376 7.509 33530 7.574 38990 7.639 41114 7.450 31898 7.515 32912 7.580 38081 7.645 40449 7.455 30798 7.521 33448 7.586 40700 7.651 37541 7.461 30963 7.527 31692 7.592 37138 7.657 37864 7.467 32091 7.533 34981 7.598 37849 7.663 38480 7.473 32533 7.539 37424 7.604 39815 7.669 39792 7.479 32702 7.544 36882 7.610 38536 7.675 39383 7.485 34550 7.550 35256 7.616 37839 7.681 37150 7.491 34142 7.556 35403 7.622 40825 7.687 40388 7.497 35358 7.562 35145 7.628 39649 7.693 37109 7.503 34096 7.568 36879 7.634 40954 7.699 36771 TIC: CO130208_12.D\data.ms DEHP 0 ug/ml time counts time counts time counts time counts 7.705 36390 7.770 41086 7.835 45833 7.901 45155 7.711 38521 7.776 42049 7.841 46257 7.907 44122 7.717 40069 7.782 40693 7.847 44515 7.912 45263 7.723 42513 7.788 41131 7.853 45090 7.918 46673 7.728 45497 7.794 42523 7.859 45387 7.924 50449 7.734 48473 7.800 40379 7.865 43384 7.930 53841 7.740 46641 7.806 43508 7.871 41405 7.936 57497 7.746 44710 7.812 41811 7.877 40831 7.942 60072 7.752 46009 7.818 43689 7.883 43535 7.948 59946 7.758 43534 7.823 43144 7.889 44357 7.954 57307 7.764 42393 7.829 44536 7.895 43688 7.960 53494 TIC: CO130208_12.D\data.ms DEHP 0 ug/ml time counts time counts time counts time counts 7.966 51162 8.031 47326 8.096 53489 8.162 54915 7.972 51898 8.037 48028 8.102 53459 8.168 55465 7.978 48477 8.043 48279 8.108 51752 8.174 53445 7.984 48916 8.049 51053 8.114 49962 8.180 52454 7.990 49175 8.055 57076 8.120 50211 8.186 54848 7.996 48281 8.061 66313 8.126 49442 8.191 54560 8.002 48831 8.067 73814 8.132 50591 8.197 57094 8.007 51127 8.073 70684 8.138 51637 8.203 56560 8.013 49270 8.079 64372 8.144 53957 8.209 61090 8.019 48070 8.085 54217 8.150 54577 8.215 61117 8.025 48053 8.091 52952 8.156 53247 8.221 58288 TIC: CO130208_12.D\data.ms DEHP 0 ug/ml time counts time counts time counts time counts 8.227 57968 8.292 62000 8.358 70411 8.423 67992 8.233 58432 8.298 61856 8.364 78659 8.429 66608 8.239 58465 8.304 60987 8.370 86403 8.435 66108 8.245 59596 8.310 60030 8.375 83917 8.441 62971 8.251 59144 8.316 59643 8.381 75002 8.447 66130 8.257 59782 8.322 61940 8.387 67713 8.453 61808 8.263 60108 8.328 61724 8.393 66871 8.459 65273 8.269 60035 8.334 63294 8.399 65973 8.464 65386 8.275 59084 8.340 62827 8.405 68131 8.470 65267 8.280 58828 8.346 62628 8.411 70418 8.476 66401 8.286 61363 8.352 63608 8.417 69202 8.482 65642 TIC: CO130208_12.D\data.ms DEHP 0 ug/ml time counts time counts time counts time counts 8.488 66229 8.553 68868 8.619 69890 8.684 75736 8.494 69810 8.559 71854 8.625 69762 8.690 75324 8.500 67147 8.565 70955 8.631 66631 8.696 79875 8.506 65473 8.571 69964 8.637 70423 8.702 78600 8.512 65156 8.577 73049 8.643 80861 8.708 79268 8.518 65488 8.583 71439 8.648 83951 8.714 83776 8.524 63314 8.589 70434 8.654 84972 8.720 82056 8.530 64123 8.595 72488 8.660 85437 8.726 77891 8.536 66307 8.601 70291 8.666 85526 8.732 76660 8.542 67319 8.607 71410 8.672 81408 8.737 75092 8.548 67247 8.613 68640 8.678 76946 8.743 77445 TIC: CO130208_12.D\data.ms DEHP 0 ug/ml time counts time counts time counts time counts 8.749 80862 8.815 79940 8.880 84118 8.945 86309 8.755 81910 8.821 83390 8.886 86338 8.951 86433 8.761 77647 8.827 84614 8.892 87373 8.957 87276 8.767 76698 8.832 84132 8.898 86513 8.963 89322 8.773 74654 8.838 86570 8.904 88550 8.969 89897 8.779 79863 8.844 83736 8.910 85935 8.975 86262 8.785 85027 8.850 81685 8.916 84525 8.981 85554 8.791 85117 8.856 81484 8.921 87126 8.987 84202 8.797 84242 8.862 80507 8.927 87271 8.993 84917 8.803 82430 8.868 83131 8.933 85790 8.999 84558 8.809 82011 8.874 80799 8.939 84053 9.005 85578 TIC: CO130208_12.D\data.ms DEHP 0 ug/ml time counts time counts time counts time counts 9.011 90951 9.076 97189 9.141 98871 9.206 90250 9.016 89616 9.082 99356 9.147 98160 9.212 87973 9.022 88867 9.088 98158 9.153 96242 9.218 95634 9.028 85886 9.094 101052 9.159 94810 9.224 109809 9.034 87424 9.100 93392 9.165 94387 9.230 119396 9.040 91211 9.105 96673 9.171 94827 9.236 120514 9.046 91766 9.111 104416 9.177 96598 9.242 108117 9.052 95405 9.117 119004 9.183 94368 9.248 99614 9.058 92814 9.123 123811 9.189 95965 9.254 96568 9.064 92647 9.129 117855 9.194 96269 9.260 91876 9.070 92212 9.135 104210 9.200 91390 9.266 93447 TIC: CO130208_12.D\data.ms DEHP 0 ug/ml time counts time counts time counts time counts 9.272 94133 9.337 96496 9.402 102128 9.468 106430 9.278 92666 9.343 95174 9.408 102911 9.473 106443 9.284 91690 9.349 95541 9.414 101801 9.479 103704 9.289 92138 9.355 96582 9.420 100318 9.485 104518 9.295 95761 9.361 98769 9.426 103213 9.491 105962 9.301 100130 9.367 96940 9.432 104206 9.497 105965 9.307 101050 9.373 98843 9.438 104131 9.503 106312 9.313 97413 9.379 97896 9.444 106420 9.509 110370 9.319 91385 9.384 99298 9.450 106678 9.515 108199 9.325 92503 9.390 96813 9.456 108487 9.521 103181 9.331 95071 9.396 101227 9.462 105267 9.527 100961 TIC: CO130208_12.D\data.ms DEHP 0 ug/ml time counts time counts time counts time counts 9.533 101775 9.598 106958 9.663 119699 9.729 124095 9.539 98666 9.604 106813 9.669 124216 9.735 124062 9.545 102788 9.610 110763 9.675 124215 9.741 130187 9.551 102841 9.616 114127 9.681 124091 9.746 125057 9.557 101594 9.622 116192 9.687 131754 9.752 123075 9.562 101014 9.628 115708 9.693 133285 9.758 118724 9.568 98891 9.634 120669 9.699 134193 9.764 114886 9.574 102430 9.640 119023 9.705 128577 9.770 114779 9.580 108865 9.646 118732 9.711 127067 9.776 113503 9.586 109584 9.652 113856 9.717 123833 9.782 107180 9.592 107292 9.657 114215 9.723 128877 9.788 113342 TIC: CO130208_12.D\data.ms DEHP 0 ug/ml time counts time counts time counts time counts 9.794 109009 9.859 120990 9.925 117805 9.990 134862 9.800 112040 9.865 124858 9.930 116886 9.996 139707 9.806 114422 9.871 123007 9.936 120502 10.002 168655 9.812 110892 9.877 120348 9.942 117802 10.008 213682 9.818 114861 9.883 120818 9.948 118938 10.014 242007 9.824 112506 9.889 120867 9.954 121027 10.020 208561 9.830 112851 9.895 122995 9.960 123512 10.025 169074 9.836 114658 9.901 115933 9.966 125958 10.031 145963 9.841 114435 9.907 112252 9.972 126262 10.037 134658 9.847 115855 9.913 115042 9.978 129017 10.043 131190 9.853 118408 9.919 115669 9.984 135841 10.049 129381 TIC: CO130208_12.D\data.ms DEHP 0 ug/ml time counts time counts time counts time counts 10.055 126287 10.120 219121 10.186 141333 10.251 201522 10.061 124350 10.126 184677 10.192 139836 10.257 191322 10.067 124080 10.132 152510 10.198 144250 10.263 171407 10.073 123896 10.138 137017 10.204 136809 10.269 160098 10.079 123353 10.144 131857 10.209 136565 10.275 163167 10.085 126011 10.150 130626 10.215 131418 10.281 158174 10.091 126913 10.156 130862 10.221 135142 10.287 158026 10.097 130100 10.162 127395 10.227 137821 10.293 159711 10.103 141163 10.168 127644 10.233 142762 10.298 161453 10.109 173878 10.174 132565 10.239 150977 10.304 160480 10.114 207541 10.180 139299 10.245 181421 10.310 164125 TIC: CO130208_12.D\data.ms DEHP 0 ug/ml time counts time counts time counts time counts 10.316 172740 10.382 194166 10.447 231474 10.512 167340 10.322 179751 10.388 172141 10.453 209330 10.518 183535 10.328 168479 10.393 166164 10.459 182571 10.524 197404 10.334 153968 10.399 164689 10.465 169150 10.530 210774 10.340 145965 10.405 164763 10.471 175244 10.536 208375 10.346 149674 10.411 171024 10.477 201077 10.542 200613 10.352 181096 10.417 180198 10.482 246144 10.548 241714 10.358 245794 10.423 194212 10.488 276723 10.554 309166 10.364 309113 10.429 200726 10.494 253340 10.560 311864 10.370 319928 10.435 216326 10.500 199097 10.566 278031 10.376 246781 10.441 229758 10.506 167866 10.571 218125 TIC: CO130208_12.D\data.ms DEHP 0 ug/ml time counts time counts time counts time counts 10.577 182844 10.643 156932 10.708 194663 10.773 362245 10.583 165112 10.649 176291 10.714 224171 10.779 381188 10.589 158753 10.655 186764 10.720 275260 10.785 409929 10.595 171938 10.661 183865 10.726 295622 10.791 419065 10.601 185834 10.666 174915 10.732 271198 10.797 347775 10.607 198023 10.672 182089 10.738 219781 10.803 241424 10.613 188933 10.678 183295 10.744 187060 10.809 182561 10.619 177745 10.684 177607 10.750 189853 10.815 166244 10.625 159881 10.690 167847 10.755 224654 10.821 158404 10.631 150835 10.696 164672 10.761 293858 10.827 158007 10.637 152968 10.702 178654 10.767 347168 10.833 150486 TIC: CO130208_12.D\data.ms DEHP 0 ug/ml time counts time counts time counts time counts 10.839 152415 10.904 190846 10.969 277689 11.034 746541 10.845 155667 10.910 184825 10.975 325189 11.040 578560 10.850 161649 10.916 186329 10.981 334744 11.046 380022 10.856 168120 10.922 184233 10.987 290979 11.052 254987 10.862 200172 10.928 180795 10.993 258211 11.058 206909 10.868 244606 10.934 177780 10.999 284550 11.064 196306 10.874 301749 10.939 178103 11.005 338171 11.070 189456 10.880 325628 10.945 171191 11.011 435641 11.076 187285 10.886 302593 10.951 175776 11.017 551891 11.082 200269 10.892 248403 10.957 195001 11.023 647712 11.088 241867 10.898 204030 10.963 220790 11.029 734542 11.094 305556 TIC: CO130208_12.D\data.ms DEHP 0 ug/ml time counts time counts time counts time counts 11.100 334691 11.165 634861 11.230 245702 11.296 495920 11.106 313062 11.171 413901 11.236 231144 11.302 376893 11.112 263857 11.177 351846 11.242 215428 11.307 277592 11.118 243814 11.183 367298 11.248 237438 11.313 258039 11.123 264855 11.189 391885 11.254 307906 11.319 245641 11.129 357906 11.195 380343 11.260 401185 11.325 225349 11.135 498855 11.201 331770 11.266 420142 11.331 211986 11.141 627474 11.207 277871 11.272 364753 11.337 207489 11.147 833041 11.213 261558 11.278 354302 11.343 211746 11.153 1.04577e+006 11.218 259538 11.284 439027 11.349 226895 11.159 964098 11.224 264299 11.290 527517 11.355 263779 TIC: CO130208_12.D\data.ms DEHP 0 ug/ml time counts time counts time counts time counts 11.361 304101 11.426 248483 11.491 248226 11.557 284887 11.367 324634 11.432 252294 11.497 260968 11.563 290826 11.373 302179 11.438 260211 11.503 289665 11.569 282020 11.379 278257 11.444 269316 11.509 289252 11.575 275241 11.385 244614 11.450 276340 11.515 265842 11.581 277236 11.391 229850 11.456 278394 11.521 257859 11.586 305467 11.397 222671 11.462 260838 11.527 256405 11.592 315109 11.402 231817 11.468 248191 11.533 254297 11.598 326608 11.408 235852 11.474 254643 11.539 266188 11.604 345477 11.414 233360 11.480 257783 11.545 275286 11.610 384569 11.420 238856 11.486 251337 11.551 292160 11.616 452790 TIC: CO130208_12.D\data.ms DEHP 0 ug/ml time counts time counts time counts time counts 11.622 528267 11.687 278320 11.753 539204 11.818 299671 11.628 588550 11.693 295622 11.759 653056 11.824 288294 11.634 625121 11.699 307213 11.764 649453 11.830 287262 11.640 563250 11.705 308224 11.770 553316 11.836 293154 11.646 467537 11.711 313796 11.776 426920 11.842 308447 11.652 408818 11.717 324336 11.782 339816 11.848 309295 11.658 398596 11.723 355152 11.788 314890 11.854 316702 11.664 373032 11.729 367654 11.794 296779 11.859 319800 11.670 319488 11.735 384376 11.800 291540 11.865 316450 11.675 281539 11.741 402485 11.806 302225 11.871 308623 11.681 280232 11.747 436734 11.812 306873 11.877 299853 TIC: CO130208_12.D\data.ms DEHP 0 ug/ml time counts time counts time counts time counts 11.883 295582 11.948 298804 12.014 329699 12.079 324017 11.889 280884 11.954 306958 12.020 320368 12.085 337519 11.895 287235 11.960 323041 12.026 313280 12.091 334593 11.901 287712 11.966 320344 12.032 305010 12.097 322506 11.907 281591 11.972 304307 12.038 301145 12.103 318612 11.913 283499 11.978 294968 12.043 297089 12.109 316386 11.919 280267 11.984 300292 12.049 298629 12.115 315125 11.925 279551 11.990 321129 12.055 302658 12.121 312009 11.931 290533 11.996 330895 12.061 301306 12.127 304969 11.937 286427 12.002 340618 12.067 303230 12.132 303776 11.943 287871 12.008 333424 12.073 307510 12.138 297844 TIC: CO130208_12.D\data.ms DEHP 0 ug/ml time counts time counts time counts time counts 12.144 299583 12.210 371937 12.275 318960 12.340 318217 12.150 303648 12.216 342069 12.281 329969 12.346 325419 12.156 291936 12.222 322554 12.287 354484 12.352 334285 12.162 299192 12.227 323356 12.293 363130 12.358 356381 12.168 297195 12.233 319745 12.299 370399 12.364 369188 12.174 296007 12.239 314460 12.305 368644 12.370 357547 12.180 296599 12.245 312169 12.311 364874 12.376 346416 12.186 306665 12.251 320279 12.316 343670 12.382 333333 12.192 330394 12.257 319144 12.322 328542 12.388 333038 12.198 378741 12.263 318184 12.328 327397 12.394 326178 12.204 394781 12.269 314725 12.334 313877 12.400 320461 TIC: CO130208_12.D\data.ms DEHP 0 ug/ml time counts time counts time counts time counts 12.406 322301 12.471 307214 12.536 313147 12.601 309041 12.411 323346 12.477 301644 12.542 319888 12.607 309753 12.417 323999 12.483 306693 12.548 321984 12.613 313201 12.423 323295 12.489 307393 12.554 320726 12.619 305525 12.429 321318 12.495 310178 12.560 313112 12.625 302104 12.435 327068 12.500 303720 12.566 311798 12.631 304999 12.441 348663 12.506 300967 12.572 318141 12.637 298745 12.447 362519 12.512 302854 12.578 313335 12.643 302787 12.453 358112 12.518 302044 12.584 315695 12.649 298055 12.459 342685 12.524 305356 12.590 319405 12.655 309760 12.465 312978 12.530 306325 12.595 308761 12.661 309376 TIC: CO130208_12.D\data.ms DEHP 0 ug/ml time counts time counts time counts time counts 12.667 302646 12.732 300214 12.797 293374 12.863 579672 12.673 296183 12.738 313551 12.803 294655 12.868 600481 12.679 295186 12.744 338198 12.809 302511 12.874 543726 12.684 299137 12.750 376926 12.815 303657 12.880 437113 12.690 292929 12.756 397639 12.821 293884 12.886 360911 12.696 290457 12.762 381845 12.827 302450 12.892 316275 12.702 290665 12.768 341255 12.833 298185 12.898 302422 12.708 289489 12.773 316405 12.839 307868 12.904 288942 12.714 285228 12.779 299271 12.845 356793 12.910 293203 12.720 296201 12.785 299547 12.851 432827 12.916 282815 12.726 297596 12.791 295773 12.857 517648 12.922 285488 TIC: CO130208_12.D\data.ms DEHP 0 ug/ml time counts time counts time counts time counts 12.928 289738 12.993 287448 13.058 274903 13.124 268756 12.934 298859 12.999 289194 13.064 274964 13.130 262512 12.940 335228 13.005 285347 13.070 279564 13.136 270581 12.946 372007 13.011 285729 13.076 279442 13.141 275937 12.952 381710 13.017 283149 13.082 286989 13.147 274304 12.957 356135 13.023 279971 13.088 285531 13.153 283648 12.963 326550 13.029 272080 13.094 280504 13.159 277427 12.969 310448 13.035 272258 13.100 285239 13.165 271538 12.975 293534 13.041 279386 13.106 271793 13.171 264026 12.981 286704 13.047 270387 13.112 267869 13.177 260542 12.987 289970 13.052 270491 13.118 266698 13.183 261992 TIC: CO130208_12.D\data.ms DEHP 0 ug/ml time counts time counts time counts time counts 13.189 264670 13.254 263924 13.320 276136 13.385 259717 13.195 263419 13.260 261364 13.325 268191 13.391 249889 13.201 254068 13.266 266737 13.331 266515 13.397 254093 13.207 257950 13.272 271273 13.337 269119 13.403 249172 13.213 261735 13.278 312293 13.343 280117 13.409 245288 13.219 262313 13.284 359744 13.349 289713 13.415 246820 13.225 257192 13.290 384724 13.355 295891 13.420 250489 13.231 253978 13.296 368361 13.361 287563 13.426 251014 13.236 258277 13.302 324990 13.367 276368 13.432 250857 13.242 259848 13.308 298477 13.373 265428 13.438 253087 13.248 262852 13.314 286472 13.379 262386 13.444 249348 TIC: CO130208_12.D\data.ms DEHP 0 ug/ml time counts time counts time counts time counts 13.450 243763 13.515 247524 13.581 257251 13.646 271254 13.456 249911 13.521 246230 13.587 267628 13.652 273740 13.462 245601 13.527 251222 13.593 334620 13.658 271722 13.468 251706 13.533 244331 13.599 611736 13.664 270495 13.474 259282 13.539 241766 13.604 1.09111e+006 13.670 264751 13.480 251070 13.545 241476 13.610 1.32366e+006 13.676 262195 13.486 251584 13.551 250689 13.616 1.06419e+006 13.682 259539 13.492 252745 13.557 245625 13.622 637324 13.688 258548 13.498 244548 13.563 247693 13.628 382051 13.693 253177 13.504 251922 13.569 249936 13.634 302332 13.699 246436 13.509 249776 13.575 254636 13.640 274216 13.705 251892 TIC: CO130208_12.D\data.ms DEHP 0 ug/ml time counts time counts time counts time counts 13.711 245176 13.777 246235 13.842 249996 13.907 274087 13.717 244429 13.782 259518 13.848 247066 13.913 251041 13.723 245429 13.788 268256 13.854 250931 13.919 243272 13.729 243493 13.794 297424 13.860 255948 13.925 246280 13.735 252674 13.800 332384 13.866 256304 13.931 240574 13.741 252511 13.806 329816 13.872 250001 13.937 242854 13.747 252982 13.812 313518 13.877 245348 13.943 240910 13.753 253017 13.818 283977 13.883 251685 13.949 244203 13.759 242274 13.824 272756 13.889 268094 13.955 242794 13.765 239204 13.830 262503 13.895 291161 13.961 245457 13.771 241448 13.836 255307 13.901 290454 13.966 250796 TIC: CO130208_12.D\data.ms DEHP 0 ug/ml time counts time counts time counts time counts 13.972 255952 14.038 281925 14.103 252532 14.168 499920 13.978 251897 14.044 260404 14.109 254659 14.174 998807 13.984 250419 14.050 253199 14.115 258085 14.180 1.71378e+006 13.990 242522 14.056 255357 14.121 247121 14.186 1.83246e+006 13.996 245834 14.061 248705 14.127 252285 14.192 1.2278e+006 14.002 244659 14.067 245281 14.133 249293 14.198 643313 14.008 249127 14.073 247443 14.139 244633 14.204 351432 14.014 276912 14.079 243921 14.145 248096 14.210 273326 14.020 325933 14.085 247397 14.150 248741 14.216 255934 14.026 344803 14.091 246471 14.156 257091 14.222 254045 14.032 327041 14.097 245763 14.162 304163 14.228 240195 TIC: CO130208_12.D\data.ms DEHP 0 ug/ml time counts time counts time counts time counts 14.234 247780 14.299 332990 14.364 260434 14.429 256755 14.240 247867 14.305 320267 14.370 257683 14.435 298635 14.245 248867 14.311 302127 14.376 255243 14.441 369012 14.251 251902 14.317 278260 14.382 248655 14.447 402609 14.257 261631 14.323 271423 14.388 244278 14.453 371024 14.263 274544 14.329 260873 14.394 242205 14.459 311121 14.269 290938 14.334 248538 14.400 248488 14.465 266291 14.275 298193 14.340 241344 14.406 250458 14.471 258208 14.281 299320 14.346 238604 14.412 254954 14.477 253040 14.287 307179 14.352 245431 14.418 255072 14.483 247567 14.293 323777 14.358 250039 14.424 252091 14.489 249014 TIC: CO130208_12.D\data.ms DEHP 0 ug/ml time counts time counts time counts time counts 14.495 248373 14.560 261768 14.625 241897 14.691 247148 14.501 248881 14.566 256879 14.631 243646 14.697 256048 14.507 259113 14.572 252620 14.637 244708 14.702 261083 14.513 265036 14.578 250826 14.643 237128 14.708 262620 14.518 268616 14.584 246526 14.649 243995 14.714 261846 14.524 257877 14.590 251213 14.655 242972 14.720 259311 14.530 262419 14.596 256870 14.661 245374 14.726 266705 14.536 261468 14.602 248662 14.667 248079 14.732 267505 14.542 257890 14.608 243596 14.673 243819 14.738 267915 14.548 260012 14.613 249805 14.679 245609 14.744 256384 14.554 257309 14.619 246405 14.685 244433 14.750 255434 TIC: CO130208_12.D\data.ms DEHP 0 ug/ml time counts time counts time counts time counts 14.756 256931 14.821 254652 14.886 242252 14.952 242783 14.762 269964 14.827 252590 14.892 250167 14.958 251155 14.768 292196 14.833 244180 14.898 251956 14.964 261129 14.774 303890 14.839 237438 14.904 251995 14.970 259303 14.780 290522 14.845 230761 14.910 244188 14.975 255325 14.786 273917 14.851 232122 14.916 246491 14.981 243626 14.791 263873 14.857 232708 14.922 240988 14.987 237365 14.797 259059 14.863 234356 14.928 241081 14.993 240333 14.803 260518 14.869 230251 14.934 237649 14.999 230246 14.809 254791 14.875 232866 14.940 234414 15.005 237785 14.815 251735 14.881 231857 14.946 239366 15.011 242086 TIC: CO130208_12.D\data.ms DEHP 0 ug/ml time counts time counts time counts time counts 15.017 246207 15.082 247150 15.148 234386 15.213 221219 15.023 258972 15.088 243920 15.154 233732 15.219 216976 15.029 258868 15.094 241367 15.159 227335 15.225 219186 15.035 253707 15.100 240126 15.165 224362 15.231 242295 15.041 241844 15.106 238462 15.171 220401 15.237 254245 15.047 233574 15.112 242564 15.177 221941 15.243 259865 15.053 237569 15.118 242005 15.183 220743 15.249 246438 15.059 241595 15.124 235190 15.189 222596 15.254 228947 15.065 248646 15.130 228974 15.195 225804 15.260 221796 15.070 248893 15.136 229408 15.201 221534 15.266 229483 15.076 249630 15.142 234565 15.207 226971 15.272 238325 TIC: CO130208_12.D\data.ms DEHP 0 ug/ml time counts time counts time counts time counts 15.278 242773 15.343 211227 15.409 201412 15.474 199873 15.284 244277 15.349 207352 15.415 207380 15.480 206889 15.290 233934 15.355 207330 15.421 207255 15.486 211715 15.296 225306 15.361 200008 15.427 203848 15.492 207516 15.302 227054 15.367 198985 15.433 210196 15.498 204743 15.308 219915 15.373 197880 15.438 207755 15.504 209888 15.314 222941 15.379 200525 15.444 200557 15.510 206319 15.320 220016 15.385 200490 15.450 205386 15.516 203382 15.326 224196 15.391 206311 15.456 202174 15.522 211064 15.332 218978 15.397 205528 15.462 197781 15.527 217749 15.338 222016 15.403 207162 15.468 196839 15.533 219490 TIC: CO130208_12.D\data.ms DEHP 0 ug/ml time counts time counts time counts time counts 15.539 219666 15.605 217356 15.670 222412 15.735 226619 15.545 215723 15.611 222619 15.676 218848 15.741 231060 15.551 230892 15.617 228422 15.682 217544 15.747 236824 15.557 235633 15.622 230048 15.688 216283 15.753 227541 15.563 231476 15.628 221968 15.694 215921 15.759 217740 15.569 227379 15.634 220981 15.700 213158 15.765 212102 15.575 213659 15.640 211041 15.706 210616 15.771 205577 15.581 207479 15.646 209491 15.711 215999 15.777 204795 15.587 205622 15.652 214313 15.717 208513 15.783 198561 15.593 204267 15.658 219872 15.723 214579 15.789 196476 15.599 218003 15.664 222370 15.729 216222 15.795 192114 TIC: CO130208_12.D\data.ms DEHP 0 ug/ml time counts time counts time counts time counts 15.801 189446 15.866 189880 15.931 185336 15.996 186883 15.806 190175 15.872 185750 15.937 182473 16.002 181118 15.812 184441 15.878 186352 15.943 181614 16.008 181058 15.818 193845 15.884 188534 15.949 182674 16.014 181756 15.824 196093 15.890 181589 15.955 184945 16.020 177201 15.830 197118 15.895 183884 15.961 182045 16.026 175701 15.836 197105 15.901 179436 15.967 184279 16.032 172529 15.842 201456 15.907 183732 15.973 185347 16.038 181155 15.848 203877 15.913 185112 15.979 193616 16.044 177251 15.854 201280 15.919 190406 15.984 196730 16.050 178586 15.860 197718 15.925 186249 15.990 194711 16.056 179902 TIC: CO130208_12.D\data.ms DEHP 0 ug/ml time counts time counts time counts time counts 16.062 178874 16.127 180303 16.192 179695 16.258 188416 16.068 186628 16.133 179418 16.198 180784 16.263 193098 16.074 193194 16.139 176616 16.204 188702 16.269 195951 16.079 188584 16.145 176948 16.210 198843 16.275 193208 16.085 193659 16.151 174829 16.216 218525 16.281 190619 16.091 188240 16.157 179954 16.222 234417 16.287 190747 16.097 186726 16.163 177994 16.228 240260 16.293 196913 16.103 189566 16.168 181992 16.234 231855 16.299 202236 16.109 189853 16.174 180456 16.240 210978 16.305 200453 16.115 185128 16.180 179242 16.246 196743 16.311 204216 16.121 183132 16.186 180648 16.252 192779 16.317 211236 TIC: CO130208_12.D\data.ms DEHP 0 ug/ml time counts time counts time counts time counts 16.323 219598 16.388 175962 16.453 167033 16.519 177576 16.329 229207 16.394 178221 16.459 174874 16.525 176487 16.335 231652 16.400 171293 16.465 174186 16.531 177706 16.341 228438 16.406 177090 16.471 171597 16.536 175630 16.347 222557 16.412 171309 16.477 170779 16.542 174999 16.352 210291 16.418 169430 16.483 174396 16.548 173539 16.358 205413 16.424 169324 16.489 182981 16.554 168621 16.364 202555 16.430 165466 16.495 183877 16.560 173129 16.370 188291 16.436 165414 16.501 184193 16.566 171987 16.376 182995 16.441 169716 16.507 183681 16.572 169666 16.382 179801 16.447 166640 16.513 177089 16.578 165657 TIC: CO130208_12.D\data.ms DEHP 0 ug/ml time counts time counts time counts time counts 16.584 177878 16.649 163350 16.715 154510 16.780 197429 16.590 185964 16.655 161602 16.720 151636 16.786 191165 16.596 182386 16.661 165010 16.726 152355 16.792 200413 16.602 186781 16.667 160248 16.732 154578 16.798 205672 16.608 177809 16.673 165147 16.738 153688 16.804 204919 16.614 178572 16.679 165550 16.744 157321 16.810 211332 16.620 172304 16.685 165131 16.750 163023 16.815 212017 16.626 167392 16.691 156499 16.756 164169 16.821 202950 16.631 164614 16.697 160509 16.762 168000 16.827 198150 16.637 166218 16.703 159129 16.768 177876 16.833 193655 16.643 167475 16.709 155514 16.774 182063 16.839 180277 TIC: CO130208_12.D\data.ms DEHP 0 ug/ml time counts time counts time counts time counts 16.845 173363 16.910 155665 16.976 165382 17.041 169393 16.851 163245 16.916 161169 16.982 166719 17.047 163659 16.857 166035 16.922 165515 16.988 165462 17.053 164211 16.863 159863 16.928 163913 16.993 163276 17.059 163608 16.869 162554 16.934 164975 16.999 168954 17.065 163550 16.875 155771 16.940 169739 17.005 166886 17.071 159573 16.881 152788 16.946 166281 17.011 163368 17.077 156774 16.887 158789 16.952 168333 17.017 166863 17.083 156289 16.893 150549 16.958 163215 17.023 164179 17.088 152238 16.899 152286 16.964 166242 17.029 160288 17.094 152591 16.904 153427 16.970 168509 17.035 160746 17.100 147232 TIC: CO130208_12.D\data.ms DEHP 0 ug/ml time counts time counts time counts time counts 17.106 153035 17.172 168237 17.237 150078 17.302 146859 17.112 157411 17.177 162600 17.243 149678 17.308 149473 17.118 164994 17.183 159049 17.249 148576 17.314 151528 17.124 169994 17.189 160469 17.255 154169 17.320 150219 17.130 175824 17.195 161362 17.261 155308 17.326 154744 17.136 187305 17.201 155028 17.267 156987 17.332 157691 17.142 191757 17.207 156173 17.272 159048 17.338 157156 17.148 188158 17.213 153986 17.278 153799 17.344 160955 17.154 183992 17.219 154215 17.284 149847 17.350 156352 17.160 176985 17.225 153351 17.290 150767 17.356 157829 17.166 170341 17.231 150115 17.296 150512 17.361 154351 TIC: CO130208_12.D\data.ms DEHP 0 ug/ml time counts time counts time counts time counts 17.367 155517 17.433 137883 17.498 133207 17.563 139206 17.373 151200 17.439 132487 17.504 129393 17.569 134511 17.379 144941 17.445 133889 17.510 131326 17.575 137195 17.385 148952 17.451 132510 17.516 132761 17.581 134371 17.391 144914 17.456 134424 17.522 129162 17.587 136025 17.397 144977 17.462 141754 17.528 134788 17.593 131048 17.403 143940 17.468 138216 17.534 131482 17.599 130940 17.409 141835 17.474 130530 17.540 133405 17.605 131492 17.415 137694 17.480 137765 17.545 136501 17.611 134338 17.421 138648 17.486 135675 17.551 135843 17.617 133809 17.427 135989 17.492 133327 17.557 131777 17.623 136785 TIC: CO130208_12.D\data.ms DEHP 0 ug/ml time counts time counts time counts time counts 17.629 128855 17.694 130976 17.759 132786 17.824 123736 17.634 131905 17.700 136683 17.765 131171 17.830 127109 17.640 131404 17.706 133184 17.771 130973 17.836 130811 17.646 132425 17.712 137375 17.777 128692 17.842 131871 17.652 136710 17.718 138280 17.783 129467 17.848 135276 17.658 138626 17.724 136953 17.789 127425 17.854 131035 17.664 140303 17.729 140520 17.795 128432 17.860 130376 17.670 135178 17.735 139819 17.801 125879 17.866 130964 17.676 133355 17.741 135478 17.807 126215 17.872 132826 17.682 134771 17.747 139948 17.813 123498 17.878 133605 17.688 136703 17.753 133954 17.819 126564 17.884 134634 TIC: CO130208_12.D\data.ms DEHP 0 ug/ml time counts time counts time counts time counts 17.890 134027 17.955 129620 18.020 132426 18.086 139576 17.896 133673 17.961 129634 18.026 136757 18.092 138726 17.902 132594 17.967 128662 18.032 141774 18.097 134691 17.908 129607 17.973 131336 18.038 144155 18.103 125259 17.913 133043 17.979 128585 18.044 145861 18.109 125222 17.919 135074 17.985 128217 18.050 149248 18.115 123549 17.925 137940 17.991 134611 18.056 151537 18.121 121645 17.931 131363 17.997 131795 18.062 156317 18.127 126636 17.937 133300 18.002 132595 18.068 155484 18.133 125201 17.943 131682 18.008 130749 18.074 158210 18.139 123026 17.949 129386 18.014 132981 18.080 148717 18.145 124486 TIC: CO130208_12.D\data.ms DEHP 0 ug/ml time counts time counts time counts time counts 18.151 121650 18.216 120361 18.281 121811 18.347 127692 18.157 116379 18.222 119062 18.287 124824 18.353 125756 18.163 116945 18.228 118309 18.293 125249 18.359 125535 18.169 116176 18.234 116362 18.299 124928 18.365 124542 18.175 117675 18.240 117533 18.305 123609 18.370 120675 18.181 114367 18.246 117003 18.311 126012 18.376 120345 18.186 117852 18.252 116433 18.317 124657 18.382 114707 18.192 113858 18.258 120087 18.323 122823 18.388 113227 18.198 114924 18.264 117124 18.329 122969 18.394 114219 18.204 116047 18.270 119237 18.335 124162 18.400 111887 18.210 117114 18.276 118142 18.341 123964 18.406 113887 TIC: CO130208_12.D\data.ms DEHP 0 ug/ml time counts time counts time counts time counts 18.412 111921 18.477 124237 18.543 110325 18.608 101059 18.418 114180 18.483 124948 18.549 108874 18.614 99125 18.424 114293 18.489 123217 18.554 107587 18.620 100147 18.430 115312 18.495 122051 18.560 102719 18.626 96513 18.436 115064 18.501 125780 18.566 104346 18.632 100213 18.442 116546 18.507 124106 18.572 107357 18.638 101068 18.448 119815 18.513 123908 18.578 106520 18.644 99835 18.454 122999 18.519 122964 18.584 106175 18.649 98811 18.460 121701 18.525 119828 18.590 104518 18.655 100052 18.465 120720 18.531 114936 18.596 101406 18.661 97802 18.471 122839 18.537 111589 18.602 100436 18.667 99098 TIC: CO130208_12.D\data.ms DEHP 0 ug/ml time counts time counts time counts time counts 18.673 100610 18.738 103455 18.804 98405 18.869 98513 18.679 102821 18.744 106363 18.810 99232 18.875 97043 18.685 104969 18.750 100857 18.816 96263 18.881 99387 18.691 99645 18.756 103517 18.822 99649 18.887 97600 18.697 103281 18.762 102264 18.828 99960 18.893 97829 18.703 102814 18.768 101189 18.833 98956 18.899 99507 18.709 103917 18.774 101051 18.839 98239 18.905 99182 18.715 103932 18.780 100770 18.845 98504 18.911 99278 18.721 105347 18.786 99127 18.851 97232 18.917 100163 18.727 101411 18.792 99227 18.857 98806 18.922 100529 18.733 101877 18.798 96296 18.863 97636 18.928 99628 TIC: CO130208_12.D\data.ms DEHP 0 ug/ml time counts time counts time counts time counts 18.934 99633 19.000 92275 19.065 97390 19.130 103253 18.940 99306 19.006 95085 19.071 94110 19.136 102688 18.946 97685 19.012 93012 19.077 98231 19.142 104088 18.952 96452 19.017 93047 19.083 93684 19.148 101036 18.958 94633 19.023 91035 19.089 97467 19.154 104450 18.964 92714 19.029 93252 19.095 94970 19.160 96545 18.970 96943 19.035 92008 19.101 98950 19.166 102475 18.976 95118 19.041 92798 19.106 97436 19.172 103163 18.982 97444 19.047 93886 19.112 99985 19.178 101057 18.988 95646 19.053 91800 19.118 102287 19.184 98677 18.994 94737 19.059 91897 19.124 102804 19.190 97713 TIC: CO130208_12.D\data.ms DEHP 0 ug/ml time counts time counts time counts time counts 19.195 99113 19.261 90422 19.326 89549 19.391 89217 19.201 97531 19.267 94301 19.332 90176 19.397 92044 19.207 98733 19.273 91354 19.338 89636 19.403 91129 19.213 95774 19.279 91828 19.344 89990 19.409 91890 19.219 94746 19.285 94363 19.350 90343 19.415 90387 19.225 94858 19.290 92171 19.356 89087 19.421 94453 19.231 94745 19.296 93526 19.362 87752 19.427 93399 19.237 97965 19.302 93393 19.368 90478 19.433 91493 19.243 93637 19.308 95935 19.374 92300 19.439 88214 19.249 92754 19.314 92334 19.379 91371 19.445 92642 19.255 92664 19.320 88936 19.385 91033 19.451 92402 TIC: CO130208_12.D\data.ms DEHP 0 ug/ml time counts time counts time counts time counts 19.457 88436 19.522 96371 19.587 93243 19.653 85361 19.463 91566 19.528 97457 19.593 91228 19.658 87442 19.469 90577 19.534 99018 19.599 91528 19.664 85745 19.474 90209 19.540 98453 19.605 90127 19.670 87527 19.480 93104 19.546 101107 19.611 89285 19.676 84456 19.486 94932 19.552 100167 19.617 89781 19.682 83932 19.492 97884 19.558 98865 19.623 89203 19.688 85386 19.498 95960 19.563 98789 19.629 89120 19.694 90302 19.504 97680 19.569 97183 19.635 86632 19.700 85001 19.510 96956 19.575 94939 19.641 87263 19.706 85200 19.516 96177 19.581 94579 19.647 86558 19.712 86385 TIC: CO130208_12.D\data.ms DEHP 0 ug/ml time counts time counts time counts time counts 19.718 88280 19.783 85253 19.848 81668 19.914 88335 19.724 83930 19.789 87573 19.854 87346 19.920 88983 19.730 85231 19.795 85657 19.860 85816 19.926 92305 19.736 81943 19.801 84844 19.866 85765 19.931 92968 19.742 85999 19.807 84209 19.872 82524 19.937 92905 19.747 84643 19.813 85687 19.878 84955 19.943 94107 19.753 82736 19.819 85449 19.884 87137 19.949 93679 19.759 84912 19.825 85349 19.890 88566 19.955 97334 19.765 84378 19.831 83568 19.896 88384 19.961 96627 19.771 83359 19.837 84251 19.902 86559 19.967 97527 19.777 82467 19.842 81961 19.908 91083 19.973 95082 TIC: CO130208_12.D\data.ms DEHP 0 ug/ml time counts time counts time counts time counts 19.979 97378 19.985 95297 19.991 97127