File: D:\DATA\20130207\CO130211_01.D Operator: PBS Date Acquired: 11 Feb 2013 12:02 Instrument: 7890A_5975C Method File: 5PSPLITLESS20.M Sample Name: DEHP 0 ug/ml Misc Info: Vial Number : 131 TIC: CO130211_01.D\data.ms DEHP 0 ug/ml time counts time counts time counts time counts 5.093 42976 5.159 49249 5.224 36000 5.289 26680 5.099 47173 5.164 46210 5.230 33897 5.295 25317 5.105 52448 5.170 43407 5.236 33602 5.301 22980 5.111 56588 5.176 42444 5.242 32929 5.307 23295 5.117 56527 5.182 40067 5.248 30608 5.313 21973 5.123 56778 5.188 38157 5.254 31438 5.319 20585 5.129 56497 5.194 35581 5.259 30695 5.325 18129 5.135 53685 5.200 34977 5.265 30400 5.331 15249 5.141 52161 5.206 33955 5.271 28749 5.337 14856 5.147 50026 5.212 32907 5.277 28109 5.343 15796 5.153 48579 5.218 33803 5.283 27369 5.348 14867 TIC: CO130211_01.D\data.ms DEHP 0 ug/ml time counts time counts time counts time counts 5.354 13673 5.420 11907 5.485 10298 5.550 10153 5.360 12453 5.426 12168 5.491 11213 5.556 9860 5.366 12534 5.432 11354 5.497 10439 5.562 9742 5.372 13380 5.438 11734 5.503 10997 5.568 10347 5.378 12877 5.443 11899 5.509 11042 5.574 12644 5.384 13705 5.449 11138 5.515 10080 5.580 12100 5.390 12333 5.455 10670 5.521 10239 5.586 13113 5.396 12632 5.461 10413 5.527 9960 5.592 12447 5.402 12282 5.467 11255 5.532 9231 5.598 11506 5.408 11706 5.473 11419 5.538 10098 5.604 12017 5.414 11585 5.479 11185 5.544 9850 5.610 11459 TIC: CO130211_01.D\data.ms DEHP 0 ug/ml time counts time counts time counts time counts 5.616 10411 5.681 9110 5.746 8606 5.811 8705 5.622 11019 5.687 9995 5.752 9016 5.817 8491 5.627 10693 5.693 9439 5.758 9826 5.823 8982 5.633 10379 5.699 8537 5.764 8707 5.829 8655 5.639 10528 5.705 9664 5.770 8669 5.835 8411 5.645 9894 5.711 10144 5.776 9432 5.841 8460 5.651 9573 5.716 9213 5.782 8624 5.847 8477 5.657 9828 5.722 8856 5.788 9238 5.853 8874 5.663 10211 5.728 9121 5.794 9554 5.859 8783 5.669 10787 5.734 8566 5.800 8572 5.865 8110 5.675 9139 5.740 7835 5.806 8682 5.871 8636 TIC: CO130211_01.D\data.ms DEHP 0 ug/ml time counts time counts time counts time counts 5.877 8597 5.942 9188 6.007 8763 6.073 8512 5.883 8801 5.948 9137 6.013 8442 6.079 8691 5.889 8337 5.954 8245 6.019 8575 6.084 8423 5.895 8246 5.960 7696 6.025 8988 6.090 8254 5.900 9862 5.966 9357 6.031 8409 6.096 8041 5.906 9379 5.972 8397 6.037 8571 6.102 8232 5.912 8992 5.978 8380 6.043 8004 6.108 8459 5.918 8841 5.984 8111 6.049 9359 6.114 8380 5.924 9121 5.990 8728 6.055 8867 6.120 7637 5.930 8407 5.995 8805 6.061 8221 6.126 8352 5.936 8538 6.001 8452 6.067 9037 6.132 8323 TIC: CO130211_01.D\data.ms DEHP 0 ug/ml time counts time counts time counts time counts 6.138 8420 6.203 8378 6.268 8466 6.334 9025 6.144 7894 6.209 7567 6.274 8405 6.340 7701 6.150 9062 6.215 8515 6.280 8271 6.346 7602 6.156 8007 6.221 8567 6.286 8162 6.352 8241 6.162 8341 6.227 8164 6.292 8553 6.357 8443 6.168 8608 6.233 8433 6.298 7688 6.363 7478 6.173 8067 6.239 8616 6.304 8320 6.369 9036 6.179 7648 6.245 8749 6.310 8150 6.375 7969 6.185 8804 6.251 8366 6.316 8047 6.381 7954 6.191 9648 6.257 8089 6.322 7949 6.387 7341 6.197 9016 6.263 7966 6.328 8050 6.393 8332 TIC: CO130211_01.D\data.ms DEHP 0 ug/ml time counts time counts time counts time counts 6.399 8053 6.464 7765 6.530 7420 6.595 7079 6.405 7482 6.470 7431 6.536 7517 6.601 7768 6.411 7890 6.476 8393 6.541 8198 6.607 7793 6.417 8956 6.482 8131 6.547 8230 6.613 8632 6.423 8523 6.488 8689 6.553 7850 6.619 7270 6.429 8325 6.494 7956 6.559 8207 6.625 7491 6.435 8023 6.500 8431 6.565 8034 6.631 7437 6.441 8572 6.506 8716 6.571 7317 6.636 7571 6.447 8205 6.512 8548 6.577 8212 6.642 8344 6.452 7854 6.518 8281 6.583 7816 6.648 7970 6.458 9014 6.524 8233 6.589 8028 6.654 8084 TIC: CO130211_01.D\data.ms DEHP 0 ug/ml time counts time counts time counts time counts 6.660 7543 6.725 19281 6.791 8363 6.856 8352 6.666 7619 6.731 21988 6.797 8500 6.862 8345 6.672 8770 6.737 22585 6.803 8879 6.868 7121 6.678 7951 6.743 21334 6.809 8355 6.874 8426 6.684 8869 6.749 17173 6.815 8261 6.880 7934 6.690 8269 6.755 13482 6.820 7691 6.886 8016 6.696 7463 6.761 10179 6.826 8953 6.892 7629 6.702 8914 6.767 9746 6.832 8477 6.898 7603 6.708 10092 6.773 9345 6.838 8481 6.904 7581 6.714 11743 6.779 7732 6.844 7576 6.909 7983 6.720 16405 6.785 7760 6.850 7238 6.915 7823 TIC: CO130211_01.D\data.ms DEHP 0 ug/ml time counts time counts time counts time counts 6.921 7335 6.987 7785 7.052 7870 7.117 8347 6.927 8118 6.993 7919 7.058 7351 7.123 8198 6.933 7771 6.998 7913 7.064 8723 7.129 7790 6.939 8057 7.004 7669 7.070 7339 7.135 8071 6.945 7523 7.010 7933 7.076 8329 7.141 8190 6.951 8529 7.016 7666 7.082 7456 7.147 7847 6.957 8584 7.022 7728 7.088 8138 7.153 8294 6.963 7799 7.028 7776 7.093 7253 7.159 8339 6.969 7696 7.034 8089 7.099 7375 7.165 7493 6.975 8375 7.040 7817 7.105 7152 7.171 8032 6.981 8096 7.046 7842 7.111 8083 7.177 8096 TIC: CO130211_01.D\data.ms DEHP 0 ug/ml time counts time counts time counts time counts 7.182 7472 7.248 8459 7.313 9029 7.378 8576 7.188 6889 7.254 7813 7.319 8086 7.384 8210 7.194 8533 7.260 7381 7.325 7241 7.390 8025 7.200 8380 7.266 7586 7.331 8043 7.396 8150 7.206 7924 7.272 7459 7.337 7946 7.402 7988 7.212 8424 7.277 7378 7.343 6961 7.408 7537 7.218 8072 7.283 7618 7.349 8088 7.414 7390 7.224 7522 7.289 8401 7.355 7522 7.420 7283 7.230 7157 7.295 8763 7.361 7363 7.426 7592 7.236 6889 7.301 7620 7.366 7484 7.432 8080 7.242 7038 7.307 8803 7.372 8310 7.438 7771 TIC: CO130211_01.D\data.ms DEHP 0 ug/ml time counts time counts time counts time counts 7.444 7520 7.509 7862 7.574 7233 7.640 8039 7.450 7903 7.515 7838 7.580 8732 7.645 8764 7.456 7811 7.521 7826 7.586 8351 7.651 8674 7.461 7967 7.527 7703 7.592 8111 7.657 8606 7.467 7428 7.533 7738 7.598 8601 7.663 8575 7.473 7562 7.539 7914 7.604 8398 7.669 9314 7.479 7733 7.545 8387 7.610 8547 7.675 8377 7.485 8988 7.550 7841 7.616 7927 7.681 7790 7.491 9505 7.556 8374 7.622 8889 7.687 8278 7.497 8324 7.562 8130 7.628 7137 7.693 8612 7.503 8100 7.568 9788 7.634 8187 7.699 8850 TIC: CO130211_01.D\data.ms DEHP 0 ug/ml time counts time counts time counts time counts 7.705 8470 7.770 8174 7.835 8562 7.901 9067 7.711 9006 7.776 8631 7.841 8638 7.907 8765 7.717 8861 7.782 7829 7.847 8299 7.913 8843 7.723 9332 7.788 8297 7.853 8543 7.918 8525 7.729 8625 7.794 9220 7.859 8862 7.924 9072 7.734 8767 7.800 8698 7.865 8976 7.930 8352 7.740 8769 7.806 8207 7.871 9791 7.936 8488 7.746 8556 7.812 8707 7.877 8320 7.942 8835 7.752 9119 7.818 8872 7.883 8716 7.948 8632 7.758 9371 7.824 8381 7.889 9590 7.954 10055 7.764 9077 7.829 8903 7.895 8721 7.960 8684 TIC: CO130211_01.D\data.ms DEHP 0 ug/ml time counts time counts time counts time counts 7.966 8339 8.031 8855 8.097 8671 8.162 9612 7.972 8175 8.037 9771 8.102 8070 8.168 9265 7.978 7547 8.043 9708 8.108 8685 8.174 9233 7.984 7657 8.049 9125 8.114 9244 8.180 9104 7.990 8965 8.055 9670 8.120 9781 8.186 9188 7.996 8818 8.061 11721 8.126 8944 8.192 9476 8.002 9077 8.067 13554 8.132 8783 8.197 9480 8.008 8719 8.073 17060 8.138 9768 8.203 9604 8.013 9129 8.079 14983 8.144 9739 8.209 9087 8.019 9621 8.085 12277 8.150 8346 8.215 8660 8.025 9320 8.091 9667 8.156 9268 8.221 8270 TIC: CO130211_01.D\data.ms DEHP 0 ug/ml time counts time counts time counts time counts 8.227 9299 8.292 8865 8.358 9408 8.423 9672 8.233 9008 8.298 9422 8.364 8974 8.429 10199 8.239 9832 8.304 8983 8.370 9891 8.435 9372 8.245 10321 8.310 8299 8.375 9312 8.441 9541 8.251 9435 8.316 9888 8.381 9751 8.447 9919 8.257 9147 8.322 8734 8.387 9221 8.453 9430 8.263 8316 8.328 9585 8.393 8981 8.459 9785 8.269 9394 8.334 9115 8.399 9510 8.465 9783 8.275 9174 8.340 9413 8.405 9804 8.470 9583 8.281 9604 8.346 9372 8.411 9797 8.476 9856 8.286 9482 8.352 9091 8.417 9737 8.482 9725 TIC: CO130211_01.D\data.ms DEHP 0 ug/ml time counts time counts time counts time counts 8.488 8559 8.554 10014 8.619 9903 8.684 9971 8.494 9605 8.559 9738 8.625 8636 8.690 9572 8.500 8729 8.565 9267 8.631 9721 8.696 9100 8.506 10294 8.571 10251 8.637 9512 8.702 9470 8.512 10049 8.577 8589 8.643 9418 8.708 10079 8.518 9004 8.583 9483 8.649 9504 8.714 9991 8.524 9599 8.589 10074 8.654 8947 8.720 8091 8.530 9628 8.595 9494 8.660 9353 8.726 9246 8.536 9010 8.601 9119 8.666 9098 8.732 9581 8.542 9410 8.607 9658 8.672 8983 8.738 9593 8.548 9361 8.613 9472 8.678 9063 8.743 10337 TIC: CO130211_01.D\data.ms DEHP 0 ug/ml time counts time counts time counts time counts 8.749 9906 8.815 9694 8.880 9864 8.945 9336 8.755 9441 8.821 9910 8.886 10174 8.951 8655 8.761 8675 8.827 9694 8.892 9808 8.957 10371 8.767 9024 8.832 9438 8.898 9364 8.963 10141 8.773 9629 8.838 10192 8.904 9458 8.969 10119 8.779 9588 8.844 9373 8.910 9736 8.975 9701 8.785 9431 8.850 9405 8.916 9721 8.981 9967 8.791 9530 8.856 9127 8.922 8886 8.987 9757 8.797 10241 8.862 9743 8.927 10294 8.993 9592 8.803 9360 8.868 9921 8.933 10041 8.999 10148 8.809 9800 8.874 9745 8.939 9661 9.005 9910 TIC: CO130211_01.D\data.ms DEHP 0 ug/ml time counts time counts time counts time counts 9.011 9350 9.076 9491 9.141 9068 9.206 10448 9.017 9575 9.082 9520 9.147 9618 9.212 9611 9.022 8919 9.088 8655 9.153 10458 9.218 9673 9.028 9174 9.094 9814 9.159 9900 9.224 11033 9.034 9541 9.100 8783 9.165 9757 9.230 12381 9.040 9089 9.106 10469 9.171 9853 9.236 13650 9.046 9556 9.111 10169 9.177 10244 9.242 13231 9.052 9439 9.117 10398 9.183 8864 9.248 12241 9.058 9655 9.123 10782 9.189 9493 9.254 10529 9.064 9494 9.129 9691 9.195 9834 9.260 9973 9.070 9953 9.135 9518 9.200 9435 9.266 9548 TIC: CO130211_01.D\data.ms DEHP 0 ug/ml time counts time counts time counts time counts 9.272 9528 9.337 9433 9.402 9875 9.468 10094 9.278 9567 9.343 10055 9.408 9605 9.474 9202 9.284 9905 9.349 10889 9.414 11346 9.479 10140 9.290 9599 9.355 10730 9.420 10584 9.485 11124 9.295 10281 9.361 10084 9.426 10758 9.491 10768 9.301 9664 9.367 10178 9.432 9765 9.497 9599 9.307 9548 9.373 9366 9.438 10672 9.503 9650 9.313 9847 9.379 10730 9.444 10138 9.509 9108 9.319 9814 9.384 9794 9.450 10296 9.515 8908 9.325 10298 9.390 10032 9.456 9657 9.521 9510 9.331 9633 9.396 10588 9.462 9203 9.527 9878 TIC: CO130211_01.D\data.ms DEHP 0 ug/ml time counts time counts time counts time counts 9.533 9784 9.598 10824 9.663 10159 9.729 10920 9.539 11221 9.604 10738 9.669 10869 9.735 10384 9.545 9878 9.610 10881 9.675 9431 9.741 11056 9.551 10384 9.616 10519 9.681 9478 9.747 10979 9.557 9961 9.622 10638 9.687 10829 9.752 10968 9.563 10209 9.628 10714 9.693 11119 9.758 10116 9.568 10145 9.634 9978 9.699 10174 9.764 10674 9.574 11113 9.640 9373 9.705 10589 9.770 11727 9.580 10809 9.646 10734 9.711 9969 9.776 11544 9.586 10398 9.652 10329 9.717 11263 9.782 10955 9.592 10943 9.658 11250 9.723 11520 9.788 10781 TIC: CO130211_01.D\data.ms DEHP 0 ug/ml time counts time counts time counts time counts 9.794 10876 9.859 10685 9.925 11489 9.990 10633 9.800 10343 9.865 10461 9.931 9965 9.996 11625 9.806 10492 9.871 10709 9.936 10601 10.002 11238 9.812 11352 9.877 10145 9.942 11369 10.008 9929 9.818 10969 9.883 10085 9.948 11512 10.014 10841 9.824 10193 9.889 10714 9.954 11037 10.020 11851 9.830 10485 9.895 11500 9.960 10876 10.026 11394 9.836 10644 9.901 10524 9.966 10942 10.031 11383 9.841 10672 9.907 10010 9.972 11066 10.037 11252 9.847 9995 9.913 11035 9.978 11658 10.043 10751 9.853 11502 9.919 10741 9.984 10965 10.049 11119 TIC: CO130211_01.D\data.ms DEHP 0 ug/ml time counts time counts time counts time counts 10.055 12460 10.120 11263 10.186 11544 10.251 13754 10.061 11529 10.126 11449 10.192 11606 10.257 12347 10.067 10675 10.132 11688 10.198 10977 10.263 11528 10.073 11659 10.138 11551 10.204 10248 10.269 12442 10.079 10976 10.144 10841 10.210 11227 10.275 12381 10.085 10902 10.150 10992 10.215 11455 10.281 12826 10.091 11816 10.156 10685 10.221 12034 10.287 12973 10.097 11592 10.162 10783 10.227 11754 10.293 12437 10.103 11478 10.168 10957 10.233 11775 10.299 11491 10.109 11106 10.174 11398 10.239 11615 10.304 11803 10.115 11543 10.180 11321 10.245 11722 10.310 11461 TIC: CO130211_01.D\data.ms DEHP 0 ug/ml time counts time counts time counts time counts 10.316 11719 10.382 11415 10.447 12334 10.512 13024 10.322 11319 10.388 11252 10.453 11690 10.518 11920 10.328 12110 10.393 11671 10.459 12920 10.524 12761 10.334 10719 10.399 11010 10.465 12553 10.530 12408 10.340 10989 10.405 11225 10.471 12388 10.536 12462 10.346 12094 10.411 11475 10.477 13133 10.542 12318 10.352 11349 10.417 12118 10.483 12145 10.548 12463 10.358 11419 10.423 12525 10.488 12039 10.554 12289 10.364 11186 10.429 12674 10.494 12581 10.560 12769 10.370 10851 10.435 12729 10.500 11474 10.566 13044 10.376 11826 10.441 13259 10.506 12512 10.572 12259 TIC: CO130211_01.D\data.ms DEHP 0 ug/ml time counts time counts time counts time counts 10.577 12797 10.643 12749 10.708 12843 10.773 11886 10.583 11399 10.649 12103 10.714 12432 10.779 12797 10.589 11329 10.655 11598 10.720 11938 10.785 11942 10.595 12961 10.661 11123 10.726 12175 10.791 12394 10.601 12090 10.667 11843 10.732 13439 10.797 11704 10.607 12295 10.672 12408 10.738 12031 10.803 12882 10.613 11714 10.678 12747 10.744 13042 10.809 11707 10.619 12105 10.684 12277 10.750 12310 10.815 11684 10.625 11154 10.690 12914 10.756 13241 10.821 13566 10.631 12404 10.696 12001 10.761 12295 10.827 13817 10.637 12453 10.702 12498 10.767 14418 10.833 14202 TIC: CO130211_01.D\data.ms DEHP 0 ug/ml time counts time counts time counts time counts 10.839 13646 10.904 13920 10.969 13261 11.035 13689 10.845 11919 10.910 14142 10.975 12608 11.040 13209 10.851 12205 10.916 13562 10.981 13225 11.046 13846 10.856 12743 10.922 13528 10.987 14204 11.052 13685 10.862 13840 10.928 12689 10.993 13541 11.058 13843 10.868 12516 10.934 13537 10.999 12742 11.064 14895 10.874 13254 10.940 13531 11.005 13095 11.070 14068 10.880 12146 10.945 12609 11.011 13337 11.076 14206 10.886 13219 10.951 13414 11.017 12629 11.082 13851 10.892 13486 10.957 11737 11.023 13914 11.088 15069 10.898 13495 10.963 13933 11.029 13438 11.094 15380 TIC: CO130211_01.D\data.ms DEHP 0 ug/ml time counts time counts time counts time counts 11.100 16560 11.165 14781 11.230 17144 11.296 15934 11.106 15465 11.171 14773 11.236 17362 11.302 14798 11.112 16935 11.177 14074 11.242 16091 11.308 15815 11.118 16672 11.183 15387 11.248 15263 11.313 15528 11.124 15018 11.189 15497 11.254 14257 11.319 14352 11.129 15638 11.195 14502 11.260 15708 11.325 14860 11.135 15724 11.201 14982 11.266 14669 11.331 14585 11.141 16008 11.207 15285 11.272 14831 11.337 15791 11.147 16225 11.213 15705 11.278 14664 11.343 15106 11.153 15371 11.219 14777 11.284 14355 11.349 15023 11.159 15186 11.224 16033 11.290 14657 11.355 16038 TIC: CO130211_01.D\data.ms DEHP 0 ug/ml time counts time counts time counts time counts 11.361 15879 11.426 14907 11.492 15109 11.557 15220 11.367 15713 11.432 15359 11.497 15943 11.563 16898 11.373 15136 11.438 14632 11.503 14698 11.569 16516 11.379 16788 11.444 15994 11.509 15341 11.575 17488 11.385 16576 11.450 15356 11.515 15413 11.581 17135 11.391 15694 11.456 15273 11.521 15902 11.586 17585 11.397 16847 11.462 16567 11.527 16485 11.592 16715 11.403 16769 11.468 16077 11.533 16546 11.598 15869 11.408 15722 11.474 17027 11.539 17256 11.604 14950 11.414 15741 11.480 15469 11.545 16829 11.610 15854 11.420 15643 11.486 15958 11.551 16224 11.616 16915 TIC: CO130211_01.D\data.ms DEHP 0 ug/ml time counts time counts time counts time counts 11.622 16432 11.687 16635 11.753 18040 11.818 18305 11.628 16649 11.693 17875 11.759 18707 11.824 18775 11.634 15784 11.699 17854 11.765 19709 11.830 17793 11.640 17062 11.705 18009 11.770 18072 11.836 18276 11.646 15634 11.711 17638 11.776 19046 11.842 17400 11.652 18091 11.717 17917 11.782 17403 11.848 16432 11.658 17288 11.723 17898 11.788 18021 11.854 18766 11.664 17323 11.729 18721 11.794 17920 11.860 17610 11.670 17008 11.735 18345 11.800 19368 11.865 17891 11.676 17510 11.741 17968 11.806 19087 11.871 19458 11.681 17617 11.747 18508 11.812 18306 11.877 18331 TIC: CO130211_01.D\data.ms DEHP 0 ug/ml time counts time counts time counts time counts 11.883 19112 11.949 19149 12.014 18598 12.079 20281 11.889 17559 11.954 19161 12.020 18759 12.085 20477 11.895 18241 11.960 19997 12.026 19009 12.091 20516 11.901 18941 11.966 19022 12.032 20343 12.097 19701 11.907 18315 11.972 19347 12.038 18717 12.103 21185 11.913 18647 11.978 18801 12.044 18575 12.109 19425 11.919 16677 11.984 18283 12.049 18591 12.115 19848 11.925 18180 11.990 18738 12.055 18095 12.121 19567 11.931 19856 11.996 18998 12.061 18062 12.127 19401 11.937 19182 12.002 18933 12.067 17688 12.133 20464 11.943 18968 12.008 19081 12.073 19539 12.138 19794 TIC: CO130211_01.D\data.ms DEHP 0 ug/ml time counts time counts time counts time counts 12.144 20240 12.210 20270 12.275 20155 12.340 20820 12.150 18853 12.216 18995 12.281 18551 12.346 20513 12.156 19387 12.222 19355 12.287 20364 12.352 20682 12.162 19702 12.228 20455 12.293 20827 12.358 21664 12.168 19911 12.233 20446 12.299 20954 12.364 21425 12.174 19719 12.239 19581 12.305 22074 12.370 20657 12.180 20729 12.245 19742 12.311 21766 12.376 20540 12.186 19820 12.251 19759 12.317 21053 12.382 19873 12.192 19310 12.257 18929 12.322 20963 12.388 21134 12.198 20515 12.263 20401 12.328 19162 12.394 20418 12.204 19720 12.269 20053 12.334 20048 12.400 21872 TIC: CO130211_01.D\data.ms DEHP 0 ug/ml time counts time counts time counts time counts 12.406 19774 12.471 21320 12.536 22360 12.601 23151 12.412 21286 12.477 20428 12.542 21832 12.607 22542 12.417 21586 12.483 21535 12.548 21682 12.613 21867 12.423 21590 12.489 21666 12.554 22421 12.619 22610 12.429 21637 12.495 20708 12.560 23771 12.625 23190 12.435 21295 12.501 21485 12.566 22649 12.631 22933 12.441 21808 12.506 21174 12.572 21245 12.637 22802 12.447 21325 12.512 21220 12.578 22619 12.643 21892 12.453 20135 12.518 21701 12.584 20610 12.649 22588 12.459 20508 12.524 21829 12.590 22706 12.655 23533 12.465 22070 12.530 23028 12.595 22150 12.661 22976 TIC: CO130211_01.D\data.ms DEHP 0 ug/ml time counts time counts time counts time counts 12.667 23322 12.732 24330 12.797 25696 12.863 24278 12.673 21816 12.738 23158 12.803 24464 12.869 25786 12.679 21997 12.744 24832 12.809 23518 12.874 27006 12.685 22422 12.750 23828 12.815 25365 12.880 26824 12.690 22117 12.756 23625 12.821 25951 12.886 27331 12.696 22789 12.762 24532 12.827 24920 12.892 26024 12.702 21535 12.768 24966 12.833 23409 12.898 26563 12.708 24144 12.774 24966 12.839 25262 12.904 24099 12.714 22892 12.779 24526 12.845 24234 12.910 24201 12.720 24124 12.785 23750 12.851 24188 12.916 25087 12.726 22647 12.791 23789 12.857 25724 12.922 24980 TIC: CO130211_01.D\data.ms DEHP 0 ug/ml time counts time counts time counts time counts 12.928 27583 12.993 27638 13.058 24752 13.124 26596 12.934 26421 12.999 26397 13.064 27023 13.130 28571 12.940 25483 13.005 25790 13.070 27357 13.136 27558 12.946 25756 13.011 25441 13.076 27483 13.142 27906 12.952 24522 13.017 25679 13.082 25847 13.147 27461 12.958 25827 13.023 25883 13.088 27930 13.153 26893 12.963 26205 13.029 27014 13.094 26961 13.159 28048 12.969 24877 13.035 27156 13.100 27769 13.165 29321 12.975 26296 13.041 28236 13.106 27043 13.171 26936 12.981 26222 13.047 25209 13.112 27717 13.177 27265 12.987 25098 13.053 26943 13.118 27887 13.183 28528 TIC: CO130211_01.D\data.ms DEHP 0 ug/ml time counts time counts time counts time counts 13.189 28694 13.254 28911 13.320 29277 13.385 30626 13.195 27822 13.260 28268 13.326 29262 13.391 29578 13.201 28294 13.266 27067 13.331 28314 13.397 30898 13.207 27135 13.272 27498 13.337 30895 13.403 29968 13.213 28998 13.278 28770 13.343 29857 13.409 30210 13.219 29152 13.284 29699 13.349 29236 13.415 30059 13.225 29107 13.290 28825 13.355 29188 13.421 29515 13.231 28371 13.296 28264 13.361 30557 13.426 30123 13.237 27902 13.302 27771 13.367 32059 13.432 32525 13.242 28546 13.308 29876 13.373 30789 13.438 31162 13.248 27208 13.314 31129 13.379 32285 13.444 31610 TIC: CO130211_01.D\data.ms DEHP 0 ug/ml time counts time counts time counts time counts 13.450 31538 13.515 33553 13.581 33128 13.646 48783 13.456 32449 13.521 32348 13.587 33017 13.652 45500 13.462 30594 13.527 31754 13.593 33052 13.658 41170 13.468 32422 13.533 31348 13.599 34261 13.664 40206 13.474 30769 13.539 32425 13.604 34653 13.670 38803 13.480 31158 13.545 31447 13.610 37864 13.676 39488 13.486 31484 13.551 31721 13.616 43620 13.682 38326 13.492 31715 13.557 31946 13.622 52667 13.688 39896 13.498 31917 13.563 32866 13.628 62276 13.694 39205 13.504 30210 13.569 33487 13.634 62604 13.699 40692 13.510 31994 13.575 32189 13.640 55776 13.705 36903 TIC: CO130211_01.D\data.ms DEHP 0 ug/ml time counts time counts time counts time counts 13.711 35607 13.777 38490 13.842 39105 13.907 62430 13.717 38189 13.783 38902 13.848 39882 13.913 63416 13.723 38802 13.788 38223 13.854 39344 13.919 58384 13.729 37079 13.794 37616 13.860 38819 13.925 52764 13.735 37683 13.800 38343 13.866 41507 13.931 47871 13.741 37324 13.806 37682 13.872 43155 13.937 45444 13.747 37512 13.812 38813 13.878 44395 13.943 45843 13.753 38177 13.818 37621 13.883 41734 13.949 42168 13.759 38353 13.824 39092 13.889 44290 13.955 44119 13.765 37127 13.830 40226 13.895 45432 13.961 45116 13.771 40016 13.836 39618 13.901 51988 13.967 42034 TIC: CO130211_01.D\data.ms DEHP 0 ug/ml time counts time counts time counts time counts 13.972 43902 14.038 94721 14.103 44418 14.168 55296 13.978 46799 14.044 82895 14.109 44763 14.174 98256 13.984 46153 14.050 69015 14.115 45225 14.180 280117 13.990 43376 14.056 59346 14.121 45675 14.186 592791 13.996 44943 14.062 57922 14.127 42225 14.192 832767 14.002 44009 14.067 54971 14.133 42859 14.198 775290 14.008 42247 14.073 51835 14.139 43441 14.204 553521 14.014 43236 14.079 47004 14.145 43934 14.210 326547 14.020 49025 14.085 45549 14.151 46931 14.216 206401 14.026 69017 14.091 47053 14.156 45870 14.222 156208 14.032 84102 14.097 45782 14.162 48950 14.228 121319 TIC: CO130211_01.D\data.ms DEHP 0 ug/ml time counts time counts time counts time counts 14.234 99944 14.299 58385 14.364 52297 14.430 53200 14.240 89916 14.305 56238 14.370 52740 14.435 51485 14.246 78363 14.311 56311 14.376 52908 14.441 53280 14.251 71774 14.317 60142 14.382 50033 14.447 57706 14.257 65465 14.323 57011 14.388 50332 14.453 65451 14.263 65589 14.329 57465 14.394 52438 14.459 77244 14.269 64965 14.335 57668 14.400 50628 14.465 93716 14.275 62442 14.340 55127 14.406 52596 14.471 95218 14.281 60433 14.346 53822 14.412 52816 14.477 90397 14.287 60448 14.352 51840 14.418 50892 14.483 80573 14.293 59243 14.358 51937 14.424 53201 14.489 75853 TIC: CO130211_01.D\data.ms DEHP 0 ug/ml time counts time counts time counts time counts 14.495 68708 14.560 63957 14.625 54740 14.691 60064 14.501 67140 14.566 63606 14.631 53939 14.697 57542 14.507 62607 14.572 60071 14.637 55706 14.703 58855 14.513 65486 14.578 58709 14.643 55288 14.708 59376 14.519 66951 14.584 59521 14.649 55430 14.714 61325 14.524 68756 14.590 54968 14.655 57289 14.720 59909 14.530 68166 14.596 54034 14.661 57465 14.726 58798 14.536 65880 14.602 53424 14.667 57720 14.732 58933 14.542 64144 14.608 55915 14.673 56413 14.738 58039 14.548 64500 14.614 57968 14.679 59280 14.744 60040 14.554 64703 14.619 53968 14.685 60488 14.750 60394 TIC: CO130211_01.D\data.ms DEHP 0 ug/ml time counts time counts time counts time counts 14.756 59563 14.821 58586 14.887 60330 14.952 60285 14.762 61388 14.827 59183 14.892 58820 14.958 61003 14.768 59390 14.833 57838 14.898 59569 14.964 63473 14.774 60779 14.839 58253 14.904 60077 14.970 62868 14.780 60796 14.845 56515 14.910 60120 14.976 61668 14.786 58063 14.851 57686 14.916 57712 14.981 62890 14.792 57367 14.857 59455 14.922 60387 14.987 62013 14.797 59489 14.863 59667 14.928 60224 14.993 64801 14.803 58280 14.869 57541 14.934 61067 14.999 61649 14.809 59820 14.875 57922 14.940 60629 15.005 62475 14.815 57077 14.881 58028 14.946 60099 15.011 62607 TIC: CO130211_01.D\data.ms DEHP 0 ug/ml time counts time counts time counts time counts 15.017 60694 15.082 62194 15.148 64577 15.213 62099 15.023 63683 15.088 60234 15.154 64013 15.219 64358 15.029 60250 15.094 63910 15.160 64367 15.225 64095 15.035 61700 15.100 63571 15.165 62909 15.231 63142 15.041 61680 15.106 60858 15.171 66159 15.237 61930 15.047 60832 15.112 63268 15.177 62483 15.243 62289 15.053 60591 15.118 61665 15.183 64457 15.249 63408 15.059 60793 15.124 62930 15.189 63178 15.255 64644 15.065 62496 15.130 62311 15.195 62681 15.260 65041 15.071 62837 15.136 64552 15.201 66160 15.266 63794 15.076 63577 15.142 64675 15.207 63947 15.272 66591 TIC: CO130211_01.D\data.ms DEHP 0 ug/ml time counts time counts time counts time counts 15.278 63807 15.344 63650 15.409 65704 15.474 64791 15.284 63051 15.349 66606 15.415 67487 15.480 67542 15.290 65234 15.355 65417 15.421 66173 15.486 65904 15.296 65328 15.361 65857 15.427 65184 15.492 67623 15.302 65838 15.367 66631 15.433 65156 15.498 68242 15.308 64578 15.373 66253 15.439 66450 15.504 65736 15.314 65302 15.379 65926 15.444 67833 15.510 65696 15.320 65315 15.385 65738 15.450 67677 15.516 66834 15.326 62880 15.391 64689 15.456 65984 15.522 66645 15.332 64054 15.397 66689 15.462 66159 15.528 70116 15.338 65762 15.403 65018 15.468 65630 15.533 65494 TIC: CO130211_01.D\data.ms DEHP 0 ug/ml time counts time counts time counts time counts 15.539 67410 15.605 68031 15.670 73976 15.735 74816 15.545 64729 15.611 67536 15.676 71945 15.741 70629 15.551 66906 15.617 69132 15.682 72869 15.747 73747 15.557 66122 15.623 69583 15.688 72163 15.753 75805 15.563 66758 15.628 69739 15.694 73387 15.759 74723 15.569 66776 15.634 73429 15.700 76193 15.765 73056 15.575 64661 15.640 69531 15.706 73643 15.771 74217 15.581 65365 15.646 69225 15.712 71502 15.777 71697 15.587 66989 15.652 69808 15.717 75550 15.783 71830 15.593 66093 15.658 69661 15.723 78541 15.789 74691 15.599 68665 15.664 72165 15.729 74006 15.795 73742 TIC: CO130211_01.D\data.ms DEHP 0 ug/ml time counts time counts time counts time counts 15.801 74693 15.866 67544 15.931 72148 15.996 68043 15.806 73106 15.872 70331 15.937 67617 16.002 69031 15.812 73413 15.878 67090 15.943 69342 16.008 70020 15.818 72950 15.884 69194 15.949 68642 16.014 69099 15.824 71640 15.890 69147 15.955 67263 16.020 69693 15.830 71037 15.896 71093 15.961 70604 16.026 68098 15.836 71782 15.901 72960 15.967 69075 16.032 69310 15.842 71399 15.907 71624 15.973 71780 16.038 69895 15.848 70179 15.913 68952 15.979 69126 16.044 70111 15.854 68939 15.919 71401 15.985 68590 16.050 69303 15.860 71188 15.925 70700 15.990 69611 16.056 68756 TIC: CO130211_01.D\data.ms DEHP 0 ug/ml time counts time counts time counts time counts 16.062 69371 16.127 71165 16.192 70714 16.258 70868 16.068 67862 16.133 70353 16.198 68064 16.264 71883 16.074 70453 16.139 71306 16.204 70553 16.269 69711 16.080 69434 16.145 71183 16.210 69460 16.275 70984 16.085 68793 16.151 71607 16.216 73376 16.281 69615 16.091 70472 16.157 71343 16.222 71616 16.287 71881 16.097 72605 16.163 70895 16.228 71871 16.293 68280 16.103 73056 16.169 70578 16.234 69920 16.299 70257 16.109 68982 16.174 71535 16.240 70102 16.305 70323 16.115 70736 16.180 70144 16.246 69130 16.311 70429 16.121 72430 16.186 72498 16.252 66946 16.317 70752 TIC: CO130211_01.D\data.ms DEHP 0 ug/ml time counts time counts time counts time counts 16.323 70483 16.388 72941 16.453 68531 16.519 67951 16.329 70885 16.394 69520 16.459 68991 16.525 69694 16.335 70233 16.400 71895 16.465 69194 16.531 67470 16.341 72813 16.406 70694 16.471 70624 16.537 68189 16.347 69671 16.412 71696 16.477 69614 16.542 67070 16.353 70932 16.418 67913 16.483 67241 16.548 68064 16.358 69528 16.424 70469 16.489 69848 16.554 70966 16.364 68833 16.430 69325 16.495 70580 16.560 69214 16.370 70704 16.436 69688 16.501 68719 16.566 66919 16.376 69801 16.442 67425 16.507 70095 16.572 65098 16.382 69554 16.448 72561 16.513 69556 16.578 69355 TIC: CO130211_01.D\data.ms DEHP 0 ug/ml time counts time counts time counts time counts 16.584 67841 16.649 67367 16.715 68342 16.780 66740 16.590 69190 16.655 67555 16.721 69565 16.786 66689 16.596 69925 16.661 68910 16.726 66090 16.792 66844 16.602 68448 16.667 68605 16.732 66879 16.798 66372 16.608 68449 16.673 65794 16.738 67115 16.804 67351 16.614 67739 16.679 67652 16.744 66200 16.810 67043 16.620 69472 16.685 67986 16.750 65967 16.815 65941 16.626 67499 16.691 67542 16.756 69439 16.821 67957 16.631 68518 16.697 69833 16.762 66422 16.827 66892 16.637 67718 16.703 65749 16.768 68634 16.833 68196 16.643 69050 16.709 67786 16.774 68205 16.839 67075 TIC: CO130211_01.D\data.ms DEHP 0 ug/ml time counts time counts time counts time counts 16.845 66346 16.910 68916 16.976 68346 17.041 67031 16.851 68730 16.916 66886 16.982 66434 17.047 66366 16.857 64034 16.922 65653 16.988 67669 17.053 65618 16.863 65466 16.928 65785 16.994 66008 17.059 64388 16.869 66734 16.934 65540 16.999 63913 17.065 66599 16.875 66436 16.940 65429 17.005 66365 17.071 65757 16.881 66184 16.946 66363 17.011 66949 17.077 65062 16.887 68529 16.952 67199 17.017 67877 17.083 66780 16.893 69895 16.958 65547 17.023 67372 17.089 66568 16.899 67502 16.964 63609 17.029 66163 17.094 67345 16.905 63794 16.970 66448 17.035 65414 17.100 63451 TIC: CO130211_01.D\data.ms DEHP 0 ug/ml time counts time counts time counts time counts 17.106 65457 17.172 65447 17.237 65419 17.302 65058 17.112 65238 17.178 66071 17.243 65016 17.308 65095 17.118 64621 17.183 64989 17.249 65959 17.314 65833 17.124 66091 17.189 65004 17.255 64004 17.320 66115 17.130 66278 17.195 65473 17.261 65751 17.326 63780 17.136 65588 17.201 64011 17.267 66777 17.332 66558 17.142 68050 17.207 65821 17.272 66990 17.338 62631 17.148 65913 17.213 68117 17.278 63038 17.344 64341 17.154 66523 17.219 67290 17.284 65366 17.350 64620 17.160 68362 17.225 65055 17.290 65128 17.356 64321 17.166 66875 17.231 65429 17.296 63184 17.362 65240 TIC: CO130211_01.D\data.ms DEHP 0 ug/ml time counts time counts time counts time counts 17.367 66544 17.433 62796 17.498 64986 17.563 63381 17.373 65725 17.439 65487 17.504 64365 17.569 63259 17.379 64778 17.445 65959 17.510 65375 17.575 64736 17.385 66354 17.451 63482 17.516 63116 17.581 64441 17.391 67169 17.457 64353 17.522 63358 17.587 64054 17.397 65623 17.462 64335 17.528 65395 17.593 65927 17.403 65209 17.468 63487 17.534 65364 17.599 63928 17.409 64997 17.474 64098 17.540 65742 17.605 62731 17.415 65884 17.480 64320 17.546 66328 17.611 62355 17.421 68424 17.486 64694 17.551 64939 17.617 63557 17.427 64385 17.492 64904 17.557 63258 17.623 62839 TIC: CO130211_01.D\data.ms DEHP 0 ug/ml time counts time counts time counts time counts 17.629 64468 17.694 63188 17.759 65754 17.824 59852 17.635 63747 17.700 63894 17.765 63849 17.830 63009 17.640 65184 17.706 62534 17.771 64103 17.836 62304 17.646 63848 17.712 62421 17.777 64719 17.842 64024 17.652 63926 17.718 63915 17.783 64545 17.848 65714 17.658 62361 17.724 64595 17.789 63166 17.854 62810 17.664 63431 17.730 64540 17.795 63593 17.860 63857 17.670 63125 17.735 62378 17.801 64266 17.866 63240 17.676 63539 17.741 64727 17.807 64416 17.872 64788 17.682 65134 17.747 62359 17.813 62593 17.878 63734 17.688 61500 17.753 63549 17.819 65413 17.884 62789 TIC: CO130211_01.D\data.ms DEHP 0 ug/ml time counts time counts time counts time counts 17.890 62691 17.955 63178 18.020 64281 18.086 62191 17.896 63827 17.961 63248 18.026 62863 18.092 60758 17.902 63148 17.967 63913 18.032 60350 18.098 61889 17.908 64215 17.973 64345 18.038 61075 18.103 62224 17.914 65054 17.979 62479 18.044 63794 18.109 62318 17.919 63501 17.985 62854 18.050 60065 18.115 61819 17.925 62129 17.991 61601 18.056 61987 18.121 61796 17.931 62812 17.997 62200 18.062 62579 18.127 62984 17.937 61582 18.003 62747 18.068 63683 18.133 62615 17.943 61931 18.008 63548 18.074 63773 18.139 61365 17.949 62692 18.014 63661 18.080 63859 18.145 61237 TIC: CO130211_01.D\data.ms DEHP 0 ug/ml time counts time counts time counts time counts 18.151 63412 18.216 61456 18.282 61738 18.347 62538 18.157 62420 18.222 60956 18.287 63401 18.353 61076 18.163 61227 18.228 62398 18.293 60553 18.359 60530 18.169 61604 18.234 63500 18.299 62988 18.365 62200 18.175 59741 18.240 62647 18.305 62039 18.371 59463 18.181 64736 18.246 62159 18.311 64330 18.376 60795 18.187 63628 18.252 61889 18.317 62317 18.382 62022 18.192 62232 18.258 63561 18.323 60021 18.388 64004 18.198 61285 18.264 61096 18.329 62440 18.394 63719 18.204 61215 18.270 64416 18.335 63834 18.400 63186 18.210 58407 18.276 60705 18.341 63487 18.406 64851 TIC: CO130211_01.D\data.ms DEHP 0 ug/ml time counts time counts time counts time counts 18.412 60088 18.477 61719 18.543 60835 18.608 60856 18.418 62273 18.483 60865 18.549 62081 18.614 60403 18.424 61120 18.489 60911 18.555 61144 18.620 61674 18.430 64218 18.495 61256 18.560 59299 18.626 59535 18.436 61012 18.501 61323 18.566 60303 18.632 61175 18.442 62432 18.507 62728 18.572 61301 18.638 60969 18.448 62416 18.513 61458 18.578 62550 18.644 60910 18.454 60571 18.519 60911 18.584 59687 18.650 62315 18.460 58780 18.525 61253 18.590 61861 18.655 61537 18.466 59798 18.531 62236 18.596 63214 18.661 62415 18.471 60289 18.537 62331 18.602 62762 18.667 62975 TIC: CO130211_01.D\data.ms DEHP 0 ug/ml time counts time counts time counts time counts 18.673 61741 18.739 61279 18.804 59904 18.869 59510 18.679 59623 18.744 61920 18.810 62052 18.875 59933 18.685 60587 18.750 60942 18.816 59277 18.881 61390 18.691 63088 18.756 60931 18.822 59705 18.887 56429 18.697 60187 18.762 60542 18.828 59408 18.893 59416 18.703 61446 18.768 60974 18.834 61609 18.899 60595 18.709 59277 18.774 61239 18.839 62512 18.905 61428 18.715 59642 18.780 60221 18.845 60186 18.911 59831 18.721 62852 18.786 63262 18.851 62081 18.917 58664 18.727 60655 18.792 62426 18.857 61925 18.923 63595 18.733 62151 18.798 62013 18.863 61039 18.928 60137 TIC: CO130211_01.D\data.ms DEHP 0 ug/ml time counts time counts time counts time counts 18.934 60055 19.000 59902 19.065 57569 19.130 61346 18.940 60731 19.006 56356 19.071 58149 19.136 60466 18.946 61781 19.012 61484 19.077 60454 19.142 59526 18.952 59255 19.017 58357 19.083 59772 19.148 58250 18.958 56560 19.023 59869 19.089 62062 19.154 62087 18.964 61139 19.029 59663 19.095 58114 19.160 60601 18.970 59643 19.035 61295 19.101 60009 19.166 59343 18.976 62185 19.041 57256 19.107 60764 19.172 61125 18.982 61059 19.047 60239 19.112 58866 19.178 61055 18.988 60973 19.053 59519 19.118 60227 19.184 59186 18.994 60071 19.059 58731 19.124 57293 19.190 60299 TIC: CO130211_01.D\data.ms DEHP 0 ug/ml time counts time counts time counts time counts 19.196 60065 19.261 59673 19.326 57001 19.391 57763 19.201 60580 19.267 61567 19.332 63035 19.397 58490 19.207 60801 19.273 61279 19.338 60313 19.403 58120 19.213 58620 19.279 58936 19.344 59341 19.409 58570 19.219 59613 19.285 60642 19.350 60114 19.415 59599 19.225 57840 19.291 61067 19.356 57764 19.421 61064 19.231 60226 19.296 60632 19.362 56903 19.427 59847 19.237 61060 19.302 58940 19.368 60559 19.433 58378 19.243 59759 19.308 59667 19.374 62798 19.439 60117 19.249 59265 19.314 60215 19.380 60997 19.445 59116 19.255 58593 19.320 59942 19.385 60617 19.451 60121 TIC: CO130211_01.D\data.ms DEHP 0 ug/ml time counts time counts time counts time counts 19.457 59350 19.522 58567 19.587 59576 19.653 58584 19.463 58437 19.528 62167 19.593 58125 19.659 58332 19.469 59442 19.534 57676 19.599 57864 19.664 59325 19.475 59001 19.540 56288 19.605 58701 19.670 57691 19.480 60653 19.546 56789 19.611 57923 19.676 57758 19.486 61450 19.552 57511 19.617 60226 19.682 57562 19.492 59485 19.558 57266 19.623 59014 19.688 58611 19.498 59394 19.564 59337 19.629 59183 19.694 60290 19.504 57417 19.569 58656 19.635 60631 19.700 58712 19.510 60370 19.575 59259 19.641 57318 19.706 58688 19.516 58316 19.581 57577 19.647 60398 19.712 60083 TIC: CO130211_01.D\data.ms DEHP 0 ug/ml time counts time counts time counts time counts 19.718 58671 19.783 55999 19.848 58098 19.914 60153 19.724 58861 19.789 57288 19.854 59465 19.920 59614 19.730 58951 19.795 57901 19.860 59176 19.926 59064 19.736 58280 19.801 60219 19.866 58674 19.932 58444 19.742 57146 19.807 56633 19.872 56821 19.937 57793 19.748 58425 19.813 59289 19.878 58921 19.943 55976 19.753 57871 19.819 59699 19.884 58768 19.949 56458 19.759 57109 19.825 58779 19.890 57733 19.955 57058 19.765 58185 19.831 56916 19.896 58836 19.961 56982 19.771 57103 19.837 59094 19.902 59237 19.967 57914 19.777 56524 19.843 57645 19.908 58009 19.973 58602 TIC: CO130211_01.D\data.ms DEHP 0 ug/ml time counts time counts time counts time counts 19.979 57474 19.985 58025 19.991 57961