INSTRUMENT CONTROL PARAMETERS: 7890A_5975C --------------------------------------------- C:\MSDCHEM\1\METHODS\10PSPLITLESS56.M Fri Jun 21 09:17:49 2013 Control Information ------- ----------- Sample Inlet : GC Injection Source : GC ALS Mass Spectrometer : Enabled No Sample Prep method has been assigned to this method. Oven Equilibration Time 0.1 min Max Temperature 325 degrees C Slow Fan Disabled Oven Program On 65 蚓 for 2 min then 6 蚓/min to 300 蚓 for 15 min Run Time 56.167 min Cryo Off Front Injector Syringe Size 10 無 Injection Volume 1 無 Solvent A Washes (PreInj) 3 Solvent A Washes (PostInj) 3 Solvent A Volume 8 無 Solvent B Washes (PreInj) 3 Solvent B Washes (PostInj) 3 Solvent B Volume 8 無 Sample Washes 1 Sample Wash Volume 8 無 Sample Pumps 6 Dwell Time (PreInj) 0 min Dwell Time (PostInj) 0 min Solvent Wash Draw Speed 300 無/min Solvent Wash Dispense Speed 6000 無/min Sample Wash Draw Speed 300 無/min Sample Wash Dispense Speed 6000 無/min Injection Dispense Speed 6000 無/min Viscosity Delay 0 sec Sample Depth 2 mm Injection Type Standard L1 Airgap 0.2 無 Sample Overlap Sample overlap is not enabled Front SS Inlet He Mode Pulsed Splitless Heater On 280 蚓 Pressure On 11.775 psi Total Flow On 19.3 mL/min Septum Purge Flow On 3 mL/min Gas Saver On 20 mL/min After 2 min Injection Pulse Pressure 10 psi Until 0.75 min Purge Flow to Split Vent 15 mL/min at 0.75 min Thermal Aux 2 (MSD Transfer Line) Heater On Temperature Program On 280 蚓 for 0 min Run Time 56.167 min Column #1 Agilent 19091S-433: HP-5ms HP-5MS 5% Phenyl Methyl Silox 325 蚓: 30 m x 250 痠 x 0.25 痠 In: Front SS Inlet He Out: Vacuum (Initial) 65 蚓 Pressure 11.775 psi Flow 1.3 mL/min Average Velocity 41.856 cm/sec Holdup Time 1.1946 min Flow Program On 1.3 mL/min for 0 min Run Time 56.167 min Signals Signal #1: Test Plot Save Off 50 Hz Signal #2: Test Plot Save Off 50 Hz Signal #3: Test Plot Save Off 50 Hz Signal #4: Test Plot Save Off 50 Hz MS ACQUISITION PARAMETERS General Information ------- ----------- Tune File : atune.u Acquistion Mode : Scan MS Information -- ----------- Solvent Delay : 10.00 min EMV Mode : Relative Relative Voltage : 0 Resulting EM Voltage : 1529 [Scan Parameters] Low Mass : 50.0 High Mass : 650.0 Threshold : 50 Sample # : 2 A/D Samples 4 [MSZones] MS Source : 230 C maximum 250 C MS Quad : 150 C maximum 200 C END OF MS ACQUISITION PARAMETERS TUNE PARAMETERS for SN: US12254A01 ----------------------------- Trace Ion Detection is OFF. EMISSION : 34.610 ENERGY : 69.922 REPELLER : 34.814 IONFOCUS : 90.157 ENTRANCE_LE : 16.000 EMVOLTS : 1529.412 Actual EMV : 1529.41 GAIN FACTOR : 4.69 AMUGAIN : 1301.000 AMUOFFSET : 122.063 FILAMENT : 1.000 DCPOLARITY : 1.000 ENTLENSOFFS : 18.322 MASSGAIN : -979.000 MASSOFFSET : -41.000 END OF TUNE PARAMETERS ------------------------------------ END OF INSTRUMENT CONTROL PARAMETERS ------------------------------------